(2S,3S)-methyl 3-[N-benzyl-N-(trimethylsiloxy)amino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

Base Information

Chemical Name:(2S,3S)-methyl 3-[N-benzyl-N-(trimethylsiloxy)amino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate
CAS No.:898232-07-0
Molecular Formula:C₂₅H₄₅NO₆Si₂
Molecular Weight:511.806
Hs Code.:

Synonyms:(2S,3S)-methyl 3-[N-benzyl-N-(trimethylsiloxy)amino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

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Chemical Property of (2S,3S)-methyl 3-[N-benzyl-N-(trimethylsiloxy)amino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

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Technology Process of (2S,3S)-methyl 3-[N-benzyl-N-(trimethylsiloxy)amino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

There total 3 articles about (2S,3S)-methyl 3-[N-benzyl-N-(trimethylsiloxy)amino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone

: 150811-50-0
(E)-((2-((tert-butyldimethylsilyl)oxy)-1-methoxyvinyl)oxy)trimethylsilane

: C₂₅H₄₅NO₆Si₂

: 898232-07-0
(2S,3S)-methyl 3-[N-benzyl-N-(trimethylsiloxy)amino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

Guidance literature:: With ytterbium(III) triflate; In dichloromethane; at -78 ℃; for 3h;
DOI:10.1021/jo060465t

Reference yield:

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone

: 150811-50-0
(E)-((2-((tert-butyldimethylsilyl)oxy)-1-methoxyvinyl)oxy)trimethylsilane

: 898232-11-6
(2R,3R)-methyl 3-[N-benzyl-N-(trimethylsiloxy)amino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

: C₂₅H₄₅NO₆Si₂

: C₂₅H₄₅NO₆Si₂

: 898232-07-0
(2S,3S)-methyl 3-[N-benzyl-N-(trimethylsiloxy)amino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 3h;
DOI:10.1021/jo060465t

Reference yield:

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone

: 150811-50-0
(E)-((2-((tert-butyldimethylsilyl)oxy)-1-methoxyvinyl)oxy)trimethylsilane

: 898232-14-9
(2S,3S)-methyl 3-[N-benzyl-hydroxyamino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

: 898232-11-6
(2R,3R)-methyl 3-[N-benzyl-N-(trimethylsiloxy)amino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

: C₂₅H₄₅NO₆Si₂

: 898232-07-0
(2S,3S)-methyl 3-[N-benzyl-N-(trimethylsiloxy)amino]-2-(tert-butyldimethylsiloxy)-3-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]propanoate

Guidance literature:: With zinc trifluoromethanesulfonate; In dichloromethane; at -78 ℃; for 3h; Further byproducts given;
DOI:10.1021/jo060465t