C₅₃H₇₃F₃N₇O₂₁P

Base Information

Chemical Name:C₅₃H₇₃F₃N₇O₂₁P
CAS No.:202464-73-1
Molecular Formula:C₅₃H₇₃F₃N₇O₂₁P
Molecular Weight:1232.17
Hs Code.:

C<sub>53</sub>H<sub>73</sub>F<sub>3</sub>N<sub>7</sub>O<sub>21</sub>P

Synonyms:C₅₃H₇₃F₃N₇O₂₁P

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Chemical Property of C₅₃H₇₃F₃N₇O₂₁P

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Technology Process of C₅₃H₇₃F₃N₇O₂₁P

There total 9 articles about C₅₃H₇₃F₃N₇O₂₁P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73089-68-6
benzyl 2-acetamido-4,6-O-benzylidene-3-O-[(R)-1-carboxyethyl]-2-deoxy-α-D-glucopyranoside

: 202464-73-1
C₅₃H₇₃F₃N₇O₂₁P

Guidance literature:: Multi-step reaction with 8 steps

1.1: 95 percent / EDCI; DMAP / CH₂Cl₂

2.1: aq. AcOH / Heating

3.1: pyridine

4.1: 53 percent / H₂; AcOH / Pd/C / 775.74 Torr

5.1: 1H-tetrazole / CH₂Cl₂ / 2 h

6.1: 760 mg / hydrogen peroxide / tetrahydrofuran; H₂O / 1.5 h / 20 °C

7.1: 95 percent / DBU / CH₂Cl₂ / 0.25 h

8.1: 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; N-hydroxysuccinimide / dimethylformamide / 2.5 h

8.2: 230 mg / N,N-diisopropylethyl amine / dimethylformamide / 16 h

With pyridine; 1H-tetrazole; dmap; 1-hydroxy-pyrrolidine-2,5-dione; hydrogen; dihydrogen peroxide; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja016082o

Reference yield:

: 917029-90-4
benzyl 2-acetamido-2-deoxy-3-O-(D-1-{[2-(phenylsulfonyl)ethoxy]carbonyl}ethyl)-α-D-glucopyranoside

: 202464-73-1
C₅₃H₇₃F₃N₇O₂₁P

Guidance literature:: Multi-step reaction with 6 steps

1.1: pyridine

2.1: 53 percent / H₂; AcOH / Pd/C / 775.74 Torr

3.1: 1H-tetrazole / CH₂Cl₂ / 2 h

4.1: 760 mg / hydrogen peroxide / tetrahydrofuran; H₂O / 1.5 h / 20 °C

5.1: 95 percent / DBU / CH₂Cl₂ / 0.25 h

6.1: 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; N-hydroxysuccinimide / dimethylformamide / 2.5 h

6.2: 230 mg / N,N-diisopropylethyl amine / dimethylformamide / 16 h

With pyridine; 1H-tetrazole; 1-hydroxy-pyrrolidine-2,5-dione; hydrogen; dihydrogen peroxide; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja016082o

Reference yield:

: 202464-70-8
benzyl 2-acetamido-4,6-O-benzylidene-2-deoxy-3-O-(D-1-{[2-(phenylsulfonyl)ethoxy]carbonyl}ethyl)-α-D-glucopyranoside

: 202464-73-1
C₅₃H₇₃F₃N₇O₂₁P

Guidance literature:: Multi-step reaction with 7 steps

1.1: aq. AcOH / Heating

2.1: pyridine

3.1: 53 percent / H₂; AcOH / Pd/C / 775.74 Torr

4.1: 1H-tetrazole / CH₂Cl₂ / 2 h

5.1: 760 mg / hydrogen peroxide / tetrahydrofuran; H₂O / 1.5 h / 20 °C

6.1: 95 percent / DBU / CH₂Cl₂ / 0.25 h

7.1: 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; N-hydroxysuccinimide / dimethylformamide / 2.5 h

7.2: 230 mg / N,N-diisopropylethyl amine / dimethylformamide / 16 h

With pyridine; 1H-tetrazole; 1-hydroxy-pyrrolidine-2,5-dione; hydrogen; dihydrogen peroxide; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja016082o