(E,E)-N,N'-(pyridine-2,6-diylbis(methanylylidene))bis(4-(benzyloxy)-2,6-dimethylaniline)

Base Information

Chemical Name:(E,E)-N,N'-(pyridine-2,6-diylbis(methanylylidene))bis(4-(benzyloxy)-2,6-dimethylaniline)
CAS No.:1307726-26-6
Molecular Formula:C₃₇H₃₅N₃O₂
Molecular Weight:553.704
Hs Code.:

Synonyms:(E,E)-N,N'-(pyridine-2,6-diylbis(methanylylidene))bis(4-(benzyloxy)-2,6-dimethylaniline)

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Chemical Property of (E,E)-N,N'-(pyridine-2,6-diylbis(methanylylidene))bis(4-(benzyloxy)-2,6-dimethylaniline)

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Technology Process of (E,E)-N,N'-(pyridine-2,6-diylbis(methanylylidene))bis(4-(benzyloxy)-2,6-dimethylaniline)

There total 3 articles about (E,E)-N,N'-(pyridine-2,6-diylbis(methanylylidene))bis(4-(benzyloxy)-2,6-dimethylaniline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 5431-44-7
2,6-Pyridinedicarboxaldehyde

: 51461-07-5
4-(benzyloxy)-2,6-dimethylaniline

: 1307726-26-6
(E,E)-N,N'-(pyridine-2,6-diylbis(methanylylidene))bis(4-(benzyloxy)-2,6-dimethylaniline)

Guidance literature:: With acetic acid; In ethanol; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol2009939

Reference yield:

: 4102-53-8
4-iodo-2,6-dimethylaniline

: 1307726-26-6
(E,E)-N,N'-(pyridine-2,6-diylbis(methanylylidene))bis(4-(benzyloxy)-2,6-dimethylaniline)

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide; 3,4,7,8-Tetramethyl-o-phenanthrolin; caesium carbonate / toluene / 0.33 h / 80 °C / Inert atmosphere

1.2: 24 h / 80 °C / Inert atmosphere

2.1: acetic acid / ethanol / 20 °C / Inert atmosphere

With copper(l) iodide; 3,4,7,8-Tetramethyl-o-phenanthrolin; caesium carbonate; acetic acid; In ethanol; toluene;
DOI:10.1021/ol2009939

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 1307726-26-6
(E,E)-N,N'-(pyridine-2,6-diylbis(methanylylidene))bis(4-(benzyloxy)-2,6-dimethylaniline)

Guidance literature:: Multi-step reaction with 3 steps

1.1: Iodine monochloride; sodium hydrogencarbonate / methanol; dichloromethane / 25 h / 20 °C / Inert atmosphere

2.1: copper(l) iodide; 3,4,7,8-Tetramethyl-o-phenanthrolin; caesium carbonate / toluene / 0.33 h / 80 °C / Inert atmosphere

2.2: 24 h / 80 °C / Inert atmosphere

3.1: acetic acid / ethanol / 20 °C / Inert atmosphere

With copper(l) iodide; 3,4,7,8-Tetramethyl-o-phenanthrolin; Iodine monochloride; sodium hydrogencarbonate; caesium carbonate; acetic acid; In methanol; ethanol; dichloromethane; toluene;
DOI:10.1021/ol2009939