(+/-)-4-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)butyl 2-(1-(2-(diethylamino) acetoxy)pentyl)benzoate

Base Information

Chemical Name:(+/-)-4-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)butyl 2-(1-(2-(diethylamino) acetoxy)pentyl)benzoate
CAS No.:1619988-56-5
Molecular Formula:C₃₁H₃₉NO₅S₃
Molecular Weight:601.852
Hs Code.:

Synonyms:(+/-)-4-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)butyl 2-(1-(2-(diethylamino) acetoxy)pentyl)benzoate

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Chemical Property of (+/-)-4-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)butyl 2-(1-(2-(diethylamino) acetoxy)pentyl)benzoate

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Technology Process of (+/-)-4-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)butyl 2-(1-(2-(diethylamino) acetoxy)pentyl)benzoate

There total 4 articles about (+/-)-4-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)butyl 2-(1-(2-(diethylamino) acetoxy)pentyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1319207-79-8
(+/-)-2-(1-(2-(diethylamino)acetoxy)pentyl)benzoic acid

: 1350433-15-6
5-(4-(4-bromobutoxy)phenyl)-3H-1,2-dithiole-3-thione

: 1619988-56-5
(+/-)-4-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)butyl 2-(1-(2-(diethylamino) acetoxy)pentyl)benzoate

Guidance literature:: With potassium carbonate; In acetone; at 65 ℃;
DOI:10.1039/c4ob00830h

Reference yield:

: 532-11-6
anethole trithione

: 1619988-56-5
(+/-)-4-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)butyl 2-(1-(2-(diethylamino) acetoxy)pentyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine hydrochloride / 0.5 h / 215 °C / Inert atmosphere

2: potassium carbonate / acetone / 65 °C / Inert atmosphere

3: potassium carbonate / acetone / 65 °C

With pyridine hydrochloride; potassium carbonate; In acetone;
DOI:10.1039/c4ob00830h

Reference yield:

: 1107060-38-7
(+/-)-2-[1-(2-chloroacetoxy)pentyl]benzoic acid

: 1619988-56-5
(+/-)-4-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)butyl 2-(1-(2-(diethylamino) acetoxy)pentyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 4 h / 65 °C

2: potassium carbonate / acetone / 65 °C

With potassium carbonate; In acetone;
DOI:10.1039/c4ob00830h