7-iodo-2-[(dimethylamino)methyleneimino]-4-benzyloxy-5-benzyloxymethyl-pyrrolo[3,2-d]pyrimidine

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Chemical Name:7-iodo-2-[(dimethylamino)methyleneimino]-4-benzyloxy-5-benzyloxymethyl-pyrrolo[3,2-d]pyrimidine
CAS No.:1446175-20-7
Molecular Formula:C₂₄H₂₄IN₅O₂
Molecular Weight:541.391
Hs Code.:

Synonyms:7-iodo-2-[(dimethylamino)methyleneimino]-4-benzyloxy-5-benzyloxymethyl-pyrrolo[3,2-d]pyrimidine

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Chemical Property of 7-iodo-2-[(dimethylamino)methyleneimino]-4-benzyloxy-5-benzyloxymethyl-pyrrolo[3,2-d]pyrimidine

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Technology Process of 7-iodo-2-[(dimethylamino)methyleneimino]-4-benzyloxy-5-benzyloxymethyl-pyrrolo[3,2-d]pyrimidine

There total 3 articles about 7-iodo-2-[(dimethylamino)methyleneimino]-4-benzyloxy-5-benzyloxymethyl-pyrrolo[3,2-d]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1446175-18-3
2-[(dimethylamino)methyleneimino]-4-benzyloxy-5-N-benzyloxymethyl-pyrrolo[3,2-d]pyrimidine

: 1446175-20-7
7-iodo-2-[(dimethylamino)methyleneimino]-4-benzyloxy-5-benzyloxymethyl-pyrrolo[3,2-d]pyrimidine

Guidance literature:: With N-iodo-succinimide; In dichloromethane; Inert atmosphere;
DOI:10.1021/jo400913k

Reference yield:

: 1446175-19-4
C₁₆H₁₇N₅O

: 1446175-20-7
7-iodo-2-[(dimethylamino)methyleneimino]-4-benzyloxy-5-benzyloxymethyl-pyrrolo[3,2-d]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

1.2: 1 h / Inert atmosphere

2.1: N-iodo-succinimide / dichloromethane / Inert atmosphere

With N-iodo-succinimide; sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/jo400913k

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 1446175-20-7
7-iodo-2-[(dimethylamino)methyleneimino]-4-benzyloxy-5-benzyloxymethyl-pyrrolo[3,2-d]pyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

1.2: 1 h / Inert atmosphere

2.1: N-iodo-succinimide / dichloromethane / Inert atmosphere

With N-iodo-succinimide; sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/jo400913k