C₂₂H₁₉N₃O₆

Base Information

Chemical Name:C₂₂H₁₉N₃O₆
CAS No.:1109237-13-9
Molecular Formula:C₂₂H₁₉N₃O₆
Molecular Weight:421.409
Hs Code.:

C<sub>22</sub>H<sub>19</sub>N<sub>3</sub>O<sub>6</sub>

Synonyms:C₂₂H₁₉N₃O₆

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Chemical Property of C₂₂H₁₉N₃O₆

Chemical Property:

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Technology Process of C₂₂H₁₉N₃O₆

There total 6 articles about C₂₂H₁₉N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1109237-13-9
C₂₂H₁₉N₃O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: tris-(o-tolyl)phosphine / palladium diacetate / N,N-dimethyl-formamide / 24 h / 130 °C / Inert atmosphere

2.1: sodium tetrahydroborate / ethanol / 20 °C

3.1: triethylamine / tetrahydrofuran / 1 h / 0 °C

4.1: sodium azide / N,N-dimethyl-formamide / 20 - 50 °C

4.2: 20 °C

5.1: hydrogenchloride / hexanes; diethyl ether / 20 °C

6.1: 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 48 h / 20 °C

7.1: trifluoroacetic acid / dichloromethane / 20 °C

With 4-methyl-morpholine; hydrogenchloride; sodium tetrahydroborate; sodium azide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; tris-(o-tolyl)phosphine; trifluoroacetic acid; palladium diacetate; In tetrahydrofuran; hexanes; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: C₁₅H₂₀O₅S

: 1109237-13-9
C₂₂H₁₉N₃O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium azide / N,N-dimethyl-formamide / 20 - 50 °C

1.2: 20 °C

2.1: hydrogenchloride / hexanes; diethyl ether / 20 °C

3.1: 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 48 h / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 20 °C

With 4-methyl-morpholine; hydrogenchloride; sodium azide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; trifluoroacetic acid; In hexanes; diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: C₁₄H₁₇N₃O₂

: 1109237-13-9
C₂₂H₁₉N₃O₆

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / hexanes; diethyl ether / 20 °C

2: 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 48 h / 20 °C

3: trifluoroacetic acid / dichloromethane / 20 °C

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; trifluoroacetic acid; In hexanes; diethyl ether; dichloromethane; N,N-dimethyl-formamide;