(2'S,2''S,4'S,4''S) 1-O,6-O-(4,4'-dimethyl-3,3',4,4',5,5',6,6'-octahydro-2,2'-bi-2H-pyran-2,2'-diyl)-2-O,3-O,4-O,5-O-tetrabenzyl-D-myo-inositol

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Chemical Name:(2'S,2''S,4'S,4''S) 1-O,6-O-(4,4'-dimethyl-3,3',4,4',5,5',6,6'-octahydro-2,2'-bi-2H-pyran-2,2'-diyl)-2-O,3-O,4-O,5-O-tetrabenzyl-D-myo-inositol
CAS No.:173397-70-1
Molecular Formula:C₄₆H₅₄O₈
Molecular Weight:734.93
Hs Code.:

Synonyms:(2'S,2''S,4'S,4''S) 1-O,6-O-(4,4'-dimethyl-3,3',4,4',5,5',6,6'-octahydro-2,2'-bi-2H-pyran-2,2'-diyl)-2-O,3-O,4-O,5-O-tetrabenzyl-D-myo-inositol

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Chemical Property of (2'S,2''S,4'S,4''S) 1-O,6-O-(4,4'-dimethyl-3,3',4,4',5,5',6,6'-octahydro-2,2'-bi-2H-pyran-2,2'-diyl)-2-O,3-O,4-O,5-O-tetrabenzyl-D-myo-inositol

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Technology Process of (2'S,2''S,4'S,4''S) 1-O,6-O-(4,4'-dimethyl-3,3',4,4',5,5',6,6'-octahydro-2,2'-bi-2H-pyran-2,2'-diyl)-2-O,3-O,4-O,5-O-tetrabenzyl-D-myo-inositol

There total 4 articles about (2'S,2''S,4'S,4''S) 1-O,6-O-(4,4'-dimethyl-3,3',4,4',5,5',6,6'-octahydro-2,2'-bi-2H-pyran-2,2'-diyl)-2-O,3-O,4-O,5-O-tetrabenzyl-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 100-39-0
benzyl bromide

: 173397-69-8
(2'S,2''S,4'S,4''S) 1-O,6-O-(4,4'-dimethyl-3,3',4,4',5,5',6,6'-octahydro-2,2'-bi-2H-pyran-2,2'-diyl)-D-myo-inositol

: 173397-70-1
(2'S,2''S,4'S,4''S) 1-O,6-O-(4,4'-dimethyl-3,3',4,4',5,5',6,6'-octahydro-2,2'-bi-2H-pyran-2,2'-diyl)-2-O,3-O,4-O,5-O-tetrabenzyl-D-myo-inositol

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(94)85337-1

Reference yield:

: 123355-55-5
2-O,5-O-dibenzoyl-myo-inositol

: 173397-70-1
(2'S,2''S,4'S,4''S) 1-O,6-O-(4,4'-dimethyl-3,3',4,4',5,5',6,6'-octahydro-2,2'-bi-2H-pyran-2,2'-diyl)-2-O,3-O,4-O,5-O-tetrabenzyl-D-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / camphorsulfonic acid / CHCl₃ / 28 h / Heating

2: 91 percent / 1percent aq. NaOH / methanol; diethyl ether / 14 h

3: 87 percent / NaH, n-Bu₄NI / dimethylformamide / 22 h / Ambient temperature

With sodium hydroxide; camphor-10-sulfonic acid; tetra-(n-butyl)ammonium iodide; sodium hydride; In methanol; diethyl ether; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/0957-4166(95)00318-J

Reference yield:

: 173397-68-7
(2'S,2''S,4'S,4''S) 2-O,5-O-dibenzoyl-1-O,6-O-(4,4'-dimethyl-3,3',4,4',5,5',6,6'-octahydro-2,2'-bi-2H-pyran-2,2'-diyl)-D-myo-inositol

: 173397-70-1
(2'S,2''S,4'S,4''S) 1-O,6-O-(4,4'-dimethyl-3,3',4,4',5,5',6,6'-octahydro-2,2'-bi-2H-pyran-2,2'-diyl)-2-O,3-O,4-O,5-O-tetrabenzyl-D-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / 1percent aq. NaOH / methanol; diethyl ether / 14 h

2: 87 percent / NaH, n-Bu₄NI / dimethylformamide / 22 h / Ambient temperature

With sodium hydroxide; tetra-(n-butyl)ammonium iodide; sodium hydride; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/0957-4166(95)00318-J