benzyl 2,3,6-tri-O-benzoyl-4-O-(2-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 2,3,6-tri-O-benzoyl-4-O-(2-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside
CAS No.:1429255-01-5
Molecular Formula:C₄₇H₄₄O₁₅
Molecular Weight:848.857
Hs Code.:

Synonyms:benzyl 2,3,6-tri-O-benzoyl-4-O-(2-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2,3,6-tri-O-benzoyl-4-O-(2-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Technology Process of benzyl 2,3,6-tri-O-benzoyl-4-O-(2-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

There total 9 articles about benzyl 2,3,6-tri-O-benzoyl-4-O-(2-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1429255-00-4
benzyl 2,3,6-tri-O-benzoyl-4-O-(2-O-benzoyl-3,4-O-isopropylidene-6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-β-D-glucopyranoside

: 1429255-01-5
benzyl 2,3,6-tri-O-benzoyl-4-O-(2-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: With water; acetic acid; at 65 ℃; for 2.5h;

Reference yield:

: C₅₀H₄₈O₁₅

: 1429255-01-5
benzyl 2,3,6-tri-O-benzoyl-4-O-(2-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: With palladium 10% on activated carbon; water; toluene-4-sulfonic acid; In methanol; for 14h; Reflux;

Reference yield:

: 1429254-98-7
benzyl 4-O-(6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-β-D-glucopyranoside

: 1429255-01-5
benzyl 2,3,6-tri-O-benzoyl-4-O-(2-O-benzoyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / water; acetonitrile / 2.5 h / 45 °C

2: dmap; pyridine / dichloromethane / 20 °C / Cooling

3: acetic acid; water / 2.5 h / 65 °C

With pyridine; dmap; water; toluene-4-sulfonic acid; acetic acid; In dichloromethane; water; acetonitrile;