benzyl 4-O-(3,4-O-isopropylidene-6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 4-O-(3,4-O-isopropylidene-6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-β-D-glucopyranoside
CAS No.:1429254-99-8
Molecular Formula:C₂₈H₄₆O₁₁Si
Molecular Weight:586.752
Hs Code.:

Synonyms:benzyl 4-O-(3,4-O-isopropylidene-6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Chemical Property of benzyl 4-O-(3,4-O-isopropylidene-6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-β-D-glucopyranoside

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Technology Process of benzyl 4-O-(3,4-O-isopropylidene-6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-β-D-glucopyranoside

There total 4 articles about benzyl 4-O-(3,4-O-isopropylidene-6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1429254-98-7
benzyl 4-O-(6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-β-D-glucopyranoside

: 77-76-9
2,2-dimethoxy-propane

: 1429254-99-8
benzyl 4-O-(3,4-O-isopropylidene-6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In water; acetonitrile; at 45 ℃; for 2.5h;

Reference yield:

: 68115-83-3
benzyl 2,3,6-tri-O-acetyl-4-O-(2,3-di-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranoside

: 1429254-99-8
benzyl 4-O-(3,4-O-isopropylidene-6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 24 h / 20 °C

2: methanol; sodium methylate / 15 h / 20 °C / pH 9

3: toluene-4-sulfonic acid / water; acetonitrile / 2.5 h / 45 °C

With 1H-imidazole; methanol; sodium methylate; toluene-4-sulfonic acid; In water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: C₃₅H₅₂O₁₆Si

: 1429254-99-8
benzyl 4-O-(3,4-O-isopropylidene-6-O-tert-butyldimethylsilyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; sodium methylate / 15 h / 20 °C / pH 9

2: toluene-4-sulfonic acid / water; acetonitrile / 2.5 h / 45 °C

With methanol; sodium methylate; toluene-4-sulfonic acid; In water; acetonitrile;