methyl-3-cyano-5-(2-cyano-2-{[4-(pentafluorothio)benzoyl]-amino}propoxy)benzoate

Base Information

Chemical Name:methyl-3-cyano-5-(2-cyano-2-{[4-(pentafluorothio)benzoyl]-amino}propoxy)benzoate
CAS No.:1046447-06-6
Molecular Formula:C₂₀H₁₆F₅N₃O₄S
Molecular Weight:489.423
Hs Code.:

Synonyms:methyl-3-cyano-5-(2-cyano-2-{[4-(pentafluorothio)benzoyl]-amino}propoxy)benzoate

Suppliers and Price of methyl-3-cyano-5-(2-cyano-2-{[4-(pentafluorothio)benzoyl]-amino}propoxy)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl-3-cyano-5-(2-cyano-2-{[4-(pentafluorothio)benzoyl]-amino}propoxy)benzoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of methyl-3-cyano-5-(2-cyano-2-{[4-(pentafluorothio)benzoyl]-amino}propoxy)benzoate

There total 7 articles about methyl-3-cyano-5-(2-cyano-2-{[4-(pentafluorothio)benzoyl]-amino}propoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 886732-29-2
methyl 3-cyano-5-fluorobenzoate

: 1046820-87-4,1046447-02-2,1046820-88-5
N-(1-cyano-2-hydroxy-1-methylethyl)-4-(pentafluorothio)benzamide

: 1046447-06-6
methyl-3-cyano-5-(2-cyano-2-{[4-(pentafluorothio)benzoyl]-amino}propoxy)benzoate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2.75h;

Reference yield:

: 1046446-99-4
pentafluoro(4-vinylphenyl)-λ⁶-sulfane

: 1046447-06-6
methyl-3-cyano-5-(2-cyano-2-{[4-(pentafluorothio)benzoyl]-amino}propoxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium periodate / ruthenium trichloride / tetrachloromethane; water; acetonitrile / 1 h / 20 °C

1.2: pH 1

2.1: thionyl chloride / 4 h / 65 °C

3.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / -10 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 2.75 h / 0 - 20 °C

With sodium periodate; thionyl chloride; sodium hydride; N-ethyl-N,N-diisopropylamine; ruthenium trichloride; In tetrahydrofuran; tetrachloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 2993-24-0
4-(pentafluorosulfanyl)aniline

: 1046447-06-6
methyl-3-cyano-5-(2-cyano-2-{[4-(pentafluorothio)benzoyl]-amino}propoxy)benzoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.03 h / 0 °C

1.2: 60 h / 0 - 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 1.5 h / 100 °C

3.1: sodium periodate / ruthenium trichloride / tetrachloromethane; water; acetonitrile / 1 h / 20 °C

3.2: pH 1

4.1: thionyl chloride / 4 h / 65 °C

5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / -10 °C

6.1: sodium hydride / N,N-dimethyl-formamide / 2.75 h / 0 - 20 °C

With hydrogenchloride; sodium periodate; thionyl chloride; sodium hydride; N-ethyl-N,N-diisopropylamine; sodium nitrite; ruthenium trichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; tetrachloromethane; water; N,N-dimethyl-formamide; acetonitrile;