16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17-one

Base Information

Chemical Name:16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17-one
CAS No.:1312542-94-1
Molecular Formula:C₃₁H₄₃ClN₂O
Molecular Weight:495.148
Hs Code.:

Synonyms:16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17-one

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Chemical Property of 16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17-one

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Technology Process of 16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17-one

There total 4 articles about 16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 109-01-3
1-methyl-piperazine

: 1312542-76-9
16-(4-chloro-benzylidene)-5α-androstan-3,17-dione

: 1312542-94-1
16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17-one

Guidance literature:: With sodium cyanoborohydride; acetic acid; In methanol; at 40 ℃; for 8h; pH=6;
DOI:10.1016/j.steroids.2011.03.015

Reference yield:

: 481-29-8
Epiandrosterone

: 1312542-94-1
16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17-one

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol / 12 h / 40 °C

2: Jones reagent / acetone / 0 °C

3: sodium cyanoborohydride; acetic acid / methanol / 8 h / 40 °C / pH 6

With Jones reagent; sodium cyanoborohydride; acetic acid; sodium hydroxide; In methanol; acetone;
DOI:10.1016/j.steroids.2011.03.015

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1312542-94-1
16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17-one

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol / 12 h / 40 °C

2: Jones reagent / acetone / 0 °C

3: sodium cyanoborohydride; acetic acid / methanol / 8 h / 40 °C / pH 6

With Jones reagent; sodium cyanoborohydride; acetic acid; sodium hydroxide; In methanol; acetone;
DOI:10.1016/j.steroids.2011.03.015