16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17β-ol

Base Information

Chemical Name:16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17β-ol
CAS No.:1312543-21-7
Molecular Formula:C₃₁H₄₅ClN₂O
Molecular Weight:497.164
Hs Code.:

Synonyms:16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17β-ol

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Chemical Property of 16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17β-ol

Chemical Property:

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Technology Process of 16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17β-ol

There total 5 articles about 16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17β-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1312542-94-1
16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17-one

: 1312543-21-7
16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17β-ol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 3h;
DOI:10.1016/j.steroids.2011.03.015

Reference yield:

: 1312542-76-9
16-(4-chloro-benzylidene)-5α-androstan-3,17-dione

: 1312543-21-7
16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17β-ol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium cyanoborohydride; acetic acid / methanol / 8 h / 40 °C / pH 6

2: sodium tetrahydroborate / methanol / 3 h / 0 °C

With sodium tetrahydroborate; sodium cyanoborohydride; acetic acid; In methanol;
DOI:10.1016/j.steroids.2011.03.015

Reference yield:

: 481-29-8
Epiandrosterone

: 1312543-21-7
16-(4-chloro-benzylidene)-3β-(4-methylpiperazinyl)-5α-androstan-17β-ol

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / methanol / 12 h / 40 °C

2: Jones reagent / acetone / 0 °C

3: sodium cyanoborohydride; acetic acid / methanol / 8 h / 40 °C / pH 6

4: sodium tetrahydroborate / methanol / 3 h / 0 °C

With sodium tetrahydroborate; Jones reagent; sodium cyanoborohydride; acetic acid; sodium hydroxide; In methanol; acetone;
DOI:10.1016/j.steroids.2011.03.015