dimethylvanadocene

Base Information

Chemical Name:dimethylvanadocene
CAS No.:62363-03-5
Molecular Formula:C₁₂H₁₆V
Molecular Weight:211.201
Hs Code.:

Synonyms:dimethylvanadocene

Suppliers and Price of dimethylvanadocene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethylvanadocene

Chemical Property:

Purity/Quality:

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Technology Process of dimethylvanadocene

There total 1 articles about dimethylvanadocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: vanadocene

: 506-82-1
dimethylcadmium

: 62363-03-5
dimethylvanadocene

: 7440-43-9
cadmium

Guidance literature:: In neat (no solvent); V-compd. added to Cd-compd. at room temp., immediate reaction; extd. (pentane);

Reference yield: 90.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 62363-03-5
dimethylvanadocene

: 1109-15-5
tris(pentafluorophenyl)borate

: (C₅H₅)2V(CH₃)(C₄H₈O)⁽¹⁺⁾*(CH₃)B(C₆F₅)3^(1-)=[(C₅H₅)2V(CH₃)(C₄H₈O)][(CH₃)B(C₆F₅)3]

Guidance literature:: In tetrahydrofuran; under Ar using Schlenk techniques; soln. of B(C6F5)3 in THF added to (C5H5)VMe2 dissolved in THF at room temp.; monitored by EPR; not isolated;
DOI:10.1021/om010894b

Reference yield: 80.0%

: 62363-03-5
dimethylvanadocene

: 75-05-8,26809-02-9
acetonitrile

: N,N-dimethylanilinium tetraphenylborate

: 169829-44-1
(C₅H₅)2V(CH₃)(CH₃CN)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[(C₅H₅)2V(CH₃)(CH₃CN)][B(C₆H₅)4]

Guidance literature:: In acetonitrile; byproducts: CH4; Ar-atmosphere; stirring (20°C, 12 h); filtering, washing (MeCN), drying (vac.); elem. anal.;
DOI:10.1021/om00010a010