1-[(2,3-dichlorophenyl)oxy]-3-((1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)amino)-2-propanol hydrochloride

Base Information

Chemical Name:1-[(2,3-dichlorophenyl)oxy]-3-((1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)amino)-2-propanol hydrochloride
CAS No.:198226-20-9
Molecular Formula:C₂₀H₂₅Cl₂NO₃*ClH
Molecular Weight:434.79
Hs Code.:

Synonyms:1-[(2,3-dichlorophenyl)oxy]-3-((1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)amino)-2-propanol hydrochloride

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Chemical Property of 1-[(2,3-dichlorophenyl)oxy]-3-((1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)amino)-2-propanol hydrochloride

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Technology Process of 1-[(2,3-dichlorophenyl)oxy]-3-((1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)amino)-2-propanol hydrochloride

There total 1 articles about 1-[(2,3-dichlorophenyl)oxy]-3-((1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)amino)-2-propanol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 1164109-79-8
(1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)(2-oxiranylmethyl)amine

: 576-24-9
2,3-dichlorophenol

: 198226-20-9
1-[(2,3-dichlorophenyl)oxy]-3-((1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)amino)-2-propanol hydrochloride

Guidance literature:: 2,3-dichlorophenol; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h; Inert atmosphere;

(1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)(2-oxiranylmethyl)amine; In N,N-dimethyl-formamide; at 100 ℃; for 20h; Further stages;
DOI:10.1021/jm900364m

Reference yield: 91.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 198226-20-9
1-[(2,3-dichlorophenyl)oxy]-3-((1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)amino)-2-propanol hydrochloride

: 1-[(2,3-dichlorophenyl)oxy]-3-[(1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)(methyl)amino]-2-propanol hydrochloride

Guidance literature:: formaldehyd; 1-[(2,3-dichlorophenyl)oxy]-3-((1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)amino)-2-propanol hydrochloride; With sodium cyanoborohydride; In methanol; water; at 20 ℃; for 120h; Inert atmosphere;

With hydrogenchloride; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jm900364m

Reference yield: 49.0%

: 198226-20-9
1-[(2,3-dichlorophenyl)oxy]-3-((1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)amino)-2-propanol hydrochloride

: 74-88-4
methyl iodide

: [3-[(2,3-dichlorophenyl)oxy]-2-(methyloxy)propyl](1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)amine hydrochloride

Guidance literature:: 1-[(2,3-dichlorophenyl)oxy]-3-((1,1-dimethyl-2-[4-(methyloxy)phenyl]ethyl)amino)-2-propanol hydrochloride; methyl iodide; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 120h; Inert atmosphere;

With hydrogenchloride; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jm900364m