1,2,2,3-Tetramethylbicyclo[1.1.0]butane

Base Information

Chemical Name:1,2,2,3-Tetramethylbicyclo[1.1.0]butane
CAS No.:32348-64-4
Molecular Formula:C₈H₁₄
Molecular Weight:110.199
Hs Code.:
NSC Number:174699
DSSTox Substance ID:DTXSID20306233
Mol file:32348-64-4.mol

Synonyms:NSC174699;32348-64-4;DTXSID20306233;NSC-174699

Suppliers and Price of 1,2,2,3-Tetramethylbicyclo[1.1.0]butane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,2,2,3-Tetramethylbicyclo[1.1.0]butane

Chemical Property:

Vapor Pressure:103mmHg at 25°C
Boiling Point:78.2°C at 760 mmHg
Density:0.919g/cm³
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:110.109550447
Heavy Atom Count:8
Complexity:141

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C2(C1(C2)C)C)C

Technology Process of 1,2,2,3-Tetramethylbicyclo[1.1.0]butane

There total 4 articles about 1,2,2,3-Tetramethylbicyclo[1.1.0]butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28569-96-2
1,2,2-Trimethylbicyclo<1.1.0>butan

: 74-88-4
methyl iodide

: 32348-64-4
1,2,2,3-tetramethyl-bicyclo[1.1.0]butane

Guidance literature:: Multistep reaction; (i) nBuLi, (ii) /BRN= 969135/;
DOI:10.1021/ja00777a601

Reference yield:

: 28569-96-2
1,2,2-trimethyl-bicyclo{1.1.0}butane

: 74-88-4
methyl iodide

: 32348-64-4
1,2,2,3-Tetramethylbicyclobutan

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; Yield given. Multistep reaction; 1.) pentane, RT, 36 h, 2.) pentane, RT, 2 h;