Technology Process of C12H15OS(1+)*C17H25F2O7S(1-)
There total 10 articles about C12H15OS(1+)*C17H25F2O7S(1-) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
chloroform; acetonitrile;
at 23 ℃;
for 23h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sulfuric acid / toluene / 2 h / 105 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 13 h / 0 - 23 °C
3: hydrogenchloride; water / acetonitrile; methanol / 6 h / 50 °C
4: toluene-4-sulfonic acid / tetrahydrofuran / 12 h / 23 °C
5: sodium tetrahydroborate / acetonitrile; water / 1 h / 0 °C
6: chloroform; acetonitrile / 23 h / 23 °C
With
hydrogenchloride; sodium tetrahydroborate; lithium aluminium tetrahydride; sulfuric acid; water; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; chloroform; water; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 12 h / 23 °C
2: sulfuric acid / toluene / 2 h / 105 °C
3: lithium aluminium tetrahydride / tetrahydrofuran / 13 h / 0 - 23 °C
4: hydrogenchloride; water / acetonitrile; methanol / 6 h / 50 °C
5: toluene-4-sulfonic acid / tetrahydrofuran / 12 h / 23 °C
6: sodium tetrahydroborate / acetonitrile; water / 1 h / 0 °C
7: chloroform; acetonitrile / 23 h / 23 °C
With
hydrogenchloride; sodium tetrahydroborate; lithium aluminium tetrahydride; sulfuric acid; water; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; chloroform; water; toluene; acetonitrile;