4-Oxoadamantane-1-carboxylic acid methyl ester

Base Information

• Chemical Name: 4-Oxoadamantane-1-carboxylic acid methyl ester
• CAS No.: 56674-88-5
• Molecular Formula: C12H16O3
• Molecular Weight: 208.25
• Hs Code.: 2918300090

Synonyms:4-Oxoadamantane-1-carboxylic acid methyl ester;

Chemical Property of 4-Oxoadamantane-1-carboxylic acid methyl ester

Chemical Property:

• Melting Point: 53-54 °C
• Boiling Point: 300.944 °C at 760 mmHg
• Flash Point: 130.423 °C
• PSA: 43.37000
• Density: 1.237 g/cm³
• LogP: 1.55480
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

99%min ^*data from raw suppliers

Methyl2-Adamantanone-5-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Oxoadamantane-1-carboxylic acid methyl ester

There total 13 articles about 4-Oxoadamantane-1-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methanol (67-56-1) + chemantane (20098-14-0) → methyl 4-oxoadamantane-1-carboxylate (56674-88-5)

Guidance literature:

chemantane; formic acid; With sulfuric acid; sulfur trioxide; at 60 ℃; for 2.33333h;

methanol; at 0 - 23 ℃; for 2h;

Reference yield: 99.0%

chemantane (20098-14-0) → methyl 4-oxoadamantane-1-carboxylate (56674-88-5)

Guidance literature:

In methanol; formic acid; dichloromethane;

Reference yield: 93.0%

methanol (67-56-1) + 4-oxoadamantane-1-carboxylic acid (56674-87-4) → methyl 4-oxoadamantane-1-carboxylate (56674-88-5)

Guidance literature:

With dmap; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Inert atmosphere;

upstream raw materials:

diazomethane

1-Adamantanecarboxylic acid

4-oxoadamantane-1-carboxylic acid

methanol

Downstream raw materials:

5-carbomethoxyadamantan-2-one ethylene ketal

methyl 4-hydroxyadamantane-1-carboxylate

C₂₀H₂₅N₃O₃

C₂₆H₂₈N₄O₄

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