α,α'-bis(3,5-bis(phenylthiamethyl)phenyloxy)-α''-(4-pyridinecarboxamido)mesitylene

Base Information

• Chemical Name: α,α'-bis(3,5-bis(phenylthiamethyl)phenyloxy)-α''-(4-pyridinecarboxamido)mesitylene
• CAS No.: 210366-74-8
• Molecular Formula: C₅₅H₄₈N₂O₃S₄
• Molecular Weight: 913.262

Synonyms:α,α'-bis(3,5-bis(phenylthiamethyl)phenyloxy)-α''-(4-pyridinecarboxamido)mesitylene

Chemical Property of α,α'-bis(3,5-bis(phenylthiamethyl)phenyloxy)-α''-(4-pyridinecarboxamido)mesitylene

Chemical Property:

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Technology Process of α,α'-bis(3,5-bis(phenylthiamethyl)phenyloxy)-α''-(4-pyridinecarboxamido)mesitylene

There total 4 articles about α,α'-bis(3,5-bis(phenylthiamethyl)phenyloxy)-α''-(4-pyridinecarboxamido)mesitylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

isonicotinoyl chloride hydrochloride (39178-35-3) + 3,5-Bis-(3,5-bis-phenylsulfanylmethyl-phenoxymethyl)-benzylamine (210366-73-7) → α,α'-bis(3,5-bis(phenylthiamethyl)phenyloxy)-α''-(4-pyridinecarboxamido)mesitylene (210366-74-8)

Guidance literature:

With triethylamine; In dichloromethane; Ambient temperature;

DOI:10.1021/ja974031e

Reference yield:

1,3,5-Tris(bromomethyl)benzene (18226-42-1) → α,α'-bis(3,5-bis(phenylthiamethyl)phenyloxy)-α''-(4-pyridinecarboxamido)mesitylene (210366-74-8)

Guidance literature:

Multi-step reaction with 4 steps

1: 47 percent / dimethylformamide / 10 h / 40 °C

2: 1.) K₂CO₃ / 1.) CH₃CN, 1 h, 2.) CH₃CN, RT, overnight

3: 99 percent / hydrazine monohydrate / tetrahydrofuran; ethanol / 50 °C

4: 79 percent / Et₃N / CH₂Cl₂ / Ambient temperature

With potassium carbonate; hydrazine hydrate; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja974031e

Reference yield:

α,α'-dibromo-α''-phthalimidomesitylene (188257-49-0) → α,α'-bis(3,5-bis(phenylthiamethyl)phenyloxy)-α''-(4-pyridinecarboxamido)mesitylene (210366-74-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) K₂CO₃ / 1.) CH₃CN, 1 h, 2.) CH₃CN, RT, overnight

2: 99 percent / hydrazine monohydrate / tetrahydrofuran; ethanol / 50 °C

3: 79 percent / Et₃N / CH₂Cl₂ / Ambient temperature

With potassium carbonate; hydrazine hydrate; triethylamine; In tetrahydrofuran; ethanol; dichloromethane;

DOI:10.1021/ja974031e

upstream raw materials:

isonicotinoyl chloride hydrochloride

3,5-Bis-(3,5-bis-phenylsulfanylmethyl-phenoxymethyl)-benzylamine

1,3,5-Tris(bromomethyl)benzene

α,α'-dibromo-α''-phthalimidomesitylene

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