tert-butyl (Z)-4,5,7-tri-O-benzyl-2,3-dideoxy-D-threo-hept-2-en-6-ulosonate

Base Information

Chemical Name:tert-butyl (Z)-4,5,7-tri-O-benzyl-2,3-dideoxy-D-threo-hept-2-en-6-ulosonate
CAS No.:101916-94-3
Molecular Formula:C₃₂H₃₆O₆
Molecular Weight:516.634
Hs Code.:

Synonyms:tert-butyl (Z)-4,5,7-tri-O-benzyl-2,3-dideoxy-D-threo-hept-2-en-6-ulosonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (Z)-4,5,7-tri-O-benzyl-2,3-dideoxy-D-threo-hept-2-en-6-ulosonate

Chemical Property:

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Technology Process of tert-butyl (Z)-4,5,7-tri-O-benzyl-2,3-dideoxy-D-threo-hept-2-en-6-ulosonate

There total 3 articles about tert-butyl (Z)-4,5,7-tri-O-benzyl-2,3-dideoxy-D-threo-hept-2-en-6-ulosonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 160549-10-0
2,3,5-tri-O-benzyl-D-arabinofuranose

: 101916-94-3
tert-butyl (Z)-4,5,7-tri-O-benzyl-2,3-dideoxy-D-threo-hept-2-en-6-ulosonate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CH₂Cl₂ / 25 °C

2: DMSO/(COCl)2, EtN₃

With oxalyl dichloride; dimethyl sulfoxide; ethyl azide; In dichloromethane;
DOI:10.1021/ja00271a049

Reference yield:

: 86302-43-4,35000-38-5
(tert-Butoxycarbonylmethylene)triphenylphosphorane

: 101916-94-3
tert-butyl (Z)-4,5,7-tri-O-benzyl-2,3-dideoxy-D-threo-hept-2-en-6-ulosonate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CH₂Cl₂ / 25 °C

2: DMSO/(COCl)2, EtN₃

With oxalyl dichloride; dimethyl sulfoxide; ethyl azide; In dichloromethane;
DOI:10.1021/ja00271a049

Reference yield:

: 221103-29-3
(E)-(4R,5R,6R)-4,5,7-Tris-benzyloxy-6-hydroxy-hept-2-enoic acid tert-butyl ester

: 101916-94-3
tert-butyl (Z)-4,5,7-tri-O-benzyl-2,3-dideoxy-D-threo-hept-2-en-6-ulosonate

: 101916-95-4
tert-butyl (E)-4,5,7-tri-O-benzyl-2,3-dideoxy-D-threo-hept-2-en-6-ulosonate

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; ethyl azide; Yield given. Yields of byproduct given;
DOI:10.1021/ja00271a049