4-dodecyloxy-2-hydroxybenzoic acid hydrazide

Base Information

• Chemical Name: 4-dodecyloxy-2-hydroxybenzoic acid hydrazide
• CAS No.: 88016-65-3
• Molecular Formula: C₁₉H₃₂N₂O₃
• Molecular Weight: 336.475
• Mol file: 88016-65-3.mol

Synonyms:4-dodecyloxy-2-hydroxybenzoic acid hydrazide

Chemical Property of 4-dodecyloxy-2-hydroxybenzoic acid hydrazide

Chemical Property:

Purity/Quality:

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Technology Process of 4-dodecyloxy-2-hydroxybenzoic acid hydrazide

There total 3 articles about 4-dodecyloxy-2-hydroxybenzoic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-Hydroxy-4-n-dodecoxybenzoesaeuremethylester (86840-98-4) → 4-dodecyloxy-2-hydroxybenzoic acid hydrazide (88016-65-3)

Guidance literature:

With hydrazine hydrate; In ethanol; water; for 8h; Heating;

Reference yield:

methyl 2,4-dihydroxybenzoate (2150-47-2) → 4-dodecyloxy-2-hydroxybenzoic acid hydrazide (88016-65-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / K₂CO₃ / acetone / 25 h / Heating

2: 90 percent / 66 percent hydrazine hydrate / ethanol; H₂O / 8 h / Heating

With potassium carbonate; hydrazine hydrate; In ethanol; water; acetone;

Reference yield:

1-dodecylbromide (143-15-7) → 4-dodecyloxy-2-hydroxybenzoic acid hydrazide (88016-65-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / K₂CO₃ / acetone / 25 h / Heating

2: 90 percent / 66 percent hydrazine hydrate / ethanol; H₂O / 8 h / Heating

With potassium carbonate; hydrazine hydrate; In ethanol; water; acetone;

upstream raw materials:

2-Hydroxy-4-n-dodecoxybenzoesaeuremethylester

methyl 2,4-dihydroxybenzoate

1-dodecylbromide