Technology Process of C27H30N8O3
There total 9 articles about C27H30N8O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C25H25N7O4;
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
at 20 ℃;
for 0.5h;
ethanamine hydrochloride;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylamine / dichloromethane / 2 h / 20 °C
2.1: 20 h / 100 °C
3.1: hydrogen / palladium 10% on activated carbon / ethanol / 6 h / 1551.49 Torr
4.1: N,N-dimethyl-formamide / 20 h / 20 °C
5.1: sodium hydroxide; water / methanol / 4 h / 60 °C
5.2: pH ~ 2
6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / 0.5 h / 20 °C
With
sodium hydroxide; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine;
palladium 10% on activated carbon;
In
methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylamine / dichloromethane / 2 h / 20 °C
2.1: 20 h / 100 °C
3.1: hydrogen / palladium 10% on activated carbon / ethanol / 6 h / 1551.49 Torr
4.1: N,N-dimethyl-formamide / 20 h / 20 °C
5.1: sodium hydroxide; water / methanol / 4 h / 60 °C
5.2: pH ~ 2
6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / 0.5 h / 20 °C
With
sodium hydroxide; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine;
palladium 10% on activated carbon;
In
methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;