(S)-((4S,5S)-4-((4-methoxybenzyl)oxy)-5-(methoxymethoxy)hept-6-enyl) 5-(methoxymethoxy)hept-6-enoate

Base Information

Chemical Name:(S)-((4S,5S)-4-((4-methoxybenzyl)oxy)-5-(methoxymethoxy)hept-6-enyl) 5-(methoxymethoxy)hept-6-enoate
CAS No.:1442433-46-6
Molecular Formula:C₂₆H₄₀O₈
Molecular Weight:480.599
Hs Code.:

Synonyms:(S)-((4S,5S)-4-((4-methoxybenzyl)oxy)-5-(methoxymethoxy)hept-6-enyl) 5-(methoxymethoxy)hept-6-enoate

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Chemical Property of (S)-((4S,5S)-4-((4-methoxybenzyl)oxy)-5-(methoxymethoxy)hept-6-enyl) 5-(methoxymethoxy)hept-6-enoate

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Technology Process of (S)-((4S,5S)-4-((4-methoxybenzyl)oxy)-5-(methoxymethoxy)hept-6-enyl) 5-(methoxymethoxy)hept-6-enoate

There total 16 articles about (S)-((4S,5S)-4-((4-methoxybenzyl)oxy)-5-(methoxymethoxy)hept-6-enyl) 5-(methoxymethoxy)hept-6-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1442433-43-3
(4S,5S)-4-((4-methoxybenzyl)oxy)-5-(methoxymethoxy)hept-6-en-1-ol

: 1442433-38-6
(S)-5-(methoxymethoxy)hept-6-enoic acid

: 1442433-46-6
(S)-((4S,5S)-4-((4-methoxybenzyl)oxy)-5-(methoxymethoxy)hept-6-enyl) 5-(methoxymethoxy)hept-6-enoate

Guidance literature:: (S)-5-(methoxymethoxy)hept-6-enoic acid; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 0 ℃; for 0.5h;

(4S,5S)-4-((4-methoxybenzyl)oxy)-5-(methoxymethoxy)hept-6-en-1-ol; In dichloromethane; at 0 - 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2013.04.069

Reference yield:

: 1442433-41-1
(5S,6S)-6-(4-methoxybenzyloxy)-12,12-dimethyl-11,11-diphenyl-5-vinyl-2,4,10-trioxa-11-silatri decane

: 1442433-46-6
(S)-((4S,5S)-4-((4-methoxybenzyl)oxy)-5-(methoxymethoxy)hept-6-enyl) 5-(methoxymethoxy)hept-6-enoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

2.1: dmap; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 0 °C

2.2: 12 h / 0 - 20 °C

With dmap; tetrabutyl ammonium fluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2013.04.069

Reference yield:

: C₉H₁₆O₃

: 1442433-46-6
(S)-((4S,5S)-4-((4-methoxybenzyl)oxy)-5-(methoxymethoxy)hept-6-enyl) 5-(methoxymethoxy)hept-6-enoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium chlorite; 2-methyl-but-2-ene; sodium dihydrogenphosphate / tetrahydrofuran; tert-butyl alcohol; water / 3 h / 0 - 20 °C

2.1: dmap; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 0 °C

2.2: 12 h / 0 - 20 °C

With dmap; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2013.04.069