1,4-Dihydro-1-(methoxycarbonyl-methyl)-2,6-dimethyl-4-(3-nitrophenyl)pyridin-3,5-dicarbonsaeuredimethylester

Base Information

Chemical Name:1,4-Dihydro-1-(methoxycarbonyl-methyl)-2,6-dimethyl-4-(3-nitrophenyl)pyridin-3,5-dicarbonsaeuredimethylester
CAS No.:173597-69-8
Molecular Formula:C₂₀H₂₂N₂O₈
Molecular Weight:418.403
Hs Code.:

Synonyms:1,4-Dihydro-1-(methoxycarbonyl-methyl)-2,6-dimethyl-4-(3-nitrophenyl)pyridin-3,5-dicarbonsaeuredimethylester

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Chemical Property of 1,4-Dihydro-1-(methoxycarbonyl-methyl)-2,6-dimethyl-4-(3-nitrophenyl)pyridin-3,5-dicarbonsaeuredimethylester

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Technology Process of 1,4-Dihydro-1-(methoxycarbonyl-methyl)-2,6-dimethyl-4-(3-nitrophenyl)pyridin-3,5-dicarbonsaeuredimethylester

There total 3 articles about 1,4-Dihydro-1-(methoxycarbonyl-methyl)-2,6-dimethyl-4-(3-nitrophenyl)pyridin-3,5-dicarbonsaeuredimethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 99-61-6
3-nitro-benzaldehyde

: 105-45-3
acetoacetic acid methyl ester

: 173597-69-8
1,4-Dihydro-1-(methoxycarbonyl-methyl)-2,6-dimethyl-4-(3-nitrophenyl)pyridin-3,5-dicarbonsaeuredimethylester

Guidance literature:: With pyridine; In methanol; for 504h; Heating;

Reference yield: 17.0%

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 89080-61-5
1,3-Diacetyl-2-(3-nitrophenyl)propan-1,3-dicarbonsaeuredimethylester

: 173597-69-8
1,4-Dihydro-1-(methoxycarbonyl-methyl)-2,6-dimethyl-4-(3-nitrophenyl)pyridin-3,5-dicarbonsaeuredimethylester

Guidance literature:: With pyridine; In methanol; for 120h; Heating;

Reference yield:

: 105-45-3
acetoacetic acid methyl ester

: 173597-69-8
1,4-Dihydro-1-(methoxycarbonyl-methyl)-2,6-dimethyl-4-(3-nitrophenyl)pyridin-3,5-dicarbonsaeuredimethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / ZnCl₂ / ethyl acetate / 1.) room temp., 15 min, 2.) 65 deg C, 6.5 h

2: 17 percent / pyridine / methanol / 120 h / Heating

With pyridine; zinc(II) chloride; In methanol; ethyl acetate;