3-(2,6,6-Trimethyl-cyclohex-2-enyl)-selenopropionic acid Se-methyl ester

Base Information

Chemical Name:3-(2,6,6-Trimethyl-cyclohex-2-enyl)-selenopropionic acid Se-methyl ester
CAS No.:176324-36-0
Molecular Formula:C₁₃H₂₂OSe
Molecular Weight:273.277
Hs Code.:

Synonyms:3-(2,6,6-Trimethyl-cyclohex-2-enyl)-selenopropionic acid Se-methyl ester

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Chemical Property of 3-(2,6,6-Trimethyl-cyclohex-2-enyl)-selenopropionic acid Se-methyl ester

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Technology Process of 3-(2,6,6-Trimethyl-cyclohex-2-enyl)-selenopropionic acid Se-methyl ester

There total 6 articles about 3-(2,6,6-Trimethyl-cyclohex-2-enyl)-selenopropionic acid Se-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 67132-62-1
dimethyl aluminum selenide

: 176324-34-8
ethyl 3-(2,6,6-trimethyl-2-cyclohexenyl)-propanoate

: 176324-36-0
3-(2,6,6-Trimethyl-cyclohex-2-enyl)-selenopropionic acid Se-methyl ester

Guidance literature:: In dichloromethane; toluene; for 1h;
DOI:10.1016/0040-4020(96)00149-4

Reference yield:

: 14505-74-9,41721-03-3,59462-59-8,432-24-6
α-cyclocitral

: 176324-36-0
3-(2,6,6-Trimethyl-cyclohex-2-enyl)-selenopropionic acid Se-methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / LiAlH₄ / diethyl ether / 0.5 h / Ambient temperature

2: 100 percent / pyridine / 48 h / 0 °C

3: 1.) Na / 1.) toluene, 2.) toluene, reflux, 24 h

4: 81 percent / aq. NaCl / dimethylsulfoxide / 22 h / Heating

5: 100 percent / CH₂Cl₂; toluene / 1 h

With pyridine; lithium aluminium tetrahydride; sodium; sodium chloride; In diethyl ether; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1016/0040-4020(96)00149-4

Reference yield:

: 126456-65-3
ethyl 3-(2,6,6-trimethyl-2-cyclohexenyl)-2-propenoate

: 176324-36-0
3-(2,6,6-Trimethyl-cyclohex-2-enyl)-selenopropionic acid Se-methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂, diethylamine / 10percent Pd/C / ethyl acetate / 2.75 h / 760 Torr

2: 100 percent / CH₂Cl₂; toluene / 1 h

With hydrogen; diethylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate; toluene;
DOI:10.1016/0040-4020(96)00149-4