Diphenylthiocarbamat des Aethyl-mercaptoacetats

Base Information

Chemical Name:Diphenylthiocarbamat des Aethyl-mercaptoacetats
CAS No.:98655-94-8
Molecular Formula:C₁₇H₁₇NO₃S
Molecular Weight:315.393
Hs Code.:

Synonyms:Diphenylthiocarbamat des Aethyl-mercaptoacetats

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Diphenylthiocarbamat des Aethyl-mercaptoacetats

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Technology Process of Diphenylthiocarbamat des Aethyl-mercaptoacetats

There total 1 articles about Diphenylthiocarbamat des Aethyl-mercaptoacetats which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 83-01-2
diphenylcarbamic chloride

: 623-51-8
ethyl 2-sulfanylacetate

: 98655-94-8
Diphenylthiocarbamat des Aethyl-mercaptoacetats

Guidance literature:: With sodium ethanolate; In ethanol; at 80 ℃; under 760.051 Torr;
DOI:10.1021/acs.orglett.8b02043

Reference yield: 74.0%

: 98655-94-8
Diphenylthiocarbamat des Aethyl-mercaptoacetats

: 6124-17-0
2-((diphenylcarbamoyl)thio)acetic acid

Guidance literature:: With potassium carbonate; In methanol; water; at 20 ℃; for 0.5h; under 760.051 Torr;
DOI:10.1021/acs.orglett.8b02043

Reference yield:

: 98655-94-8
Diphenylthiocarbamat des Aethyl-mercaptoacetats

: 122-39-4
diphenylamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / methanol; water / 0.5 h / 20 °C / 760.05 Torr

2.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 1 h / 20 °C / 760.05 Torr / Inert atmosphere

3.1: dichloromethane / 4 h / -20 - 20 °C / 760.05 Torr / Inert atmosphere

3.2: 0.33 h / 0 °C / 760.05 Torr / Inert atmosphere

3.3: 0.5 h / 760.05 Torr / Inert atmosphere

4.1: aluminum (III) chloride / dichloromethane / 0.5 h / 20 °C / 760.05 Torr / Inert atmosphere

4.2: 760.05 Torr / Inert atmosphere

5.1: methanol / Irradiation

With aluminum (III) chloride; oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In methanol; dichloromethane; water;
DOI:10.1021/acs.orglett.8b02043