1,3-dimethyl-N-(4-(methoxycarbonyl)phenyl)-1H-pyrazolo[3,4-b]quinolin-4-amine

Base Information

• Chemical Name: 1,3-dimethyl-N-(4-(methoxycarbonyl)phenyl)-1H-pyrazolo[3,4-b]quinolin-4-amine
• CAS No.: 884316-33-0
• Molecular Formula: C₂₀H₁₈N₄O₂
• Molecular Weight: 346.389

Synonyms:1,3-dimethyl-N-(4-(methoxycarbonyl)phenyl)-1H-pyrazolo[3,4-b]quinolin-4-amine

Chemical Property of 1,3-dimethyl-N-(4-(methoxycarbonyl)phenyl)-1H-pyrazolo[3,4-b]quinolin-4-amine

Chemical Property:

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Technology Process of 1,3-dimethyl-N-(4-(methoxycarbonyl)phenyl)-1H-pyrazolo[3,4-b]quinolin-4-amine

There total 1 articles about 1,3-dimethyl-N-(4-(methoxycarbonyl)phenyl)-1H-pyrazolo[3,4-b]quinolin-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

4-chloro-1,3-dimethyl-1H-pyrazolo[3,4-b]quinoline (24158-31-4) + 4-methoxycarbonyl aniline (619-45-4) → 1,3-dimethyl-N-(4-(methoxycarbonyl)phenyl)-1H-pyrazolo[3,4-b]quinolin-4-amine (884316-33-0)

Guidance literature:

With phenol; at 100 ℃; for 4h;

Reference yield: 80.0%

1,3-dimethyl-N-(4-(methoxycarbonyl)phenyl)-1H-pyrazolo[3,4-b]quinolin-4-amine (884316-33-0) + methyl iodide (74-88-4) → 1,3-dimethyl-N-methyl-N-(4-methoxycarbonylphenyl)-1H-pyrazolo[3,4-b]quinolin-4-amine

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 0.5h;

Reference yield:

1,3-dimethyl-N-(4-(methoxycarbonyl)phenyl)-1H-pyrazolo[3,4-b]quinolin-4-amine (884316-33-0) → N-(4-carboxyphenyl)-1,3-dimethyl-1H-pyrazolo[3,4-b]quinolin-4-amine

Guidance literature:

With sodium hydroxide; In methanol; for 4h; Heating;

DOI:10.1016/j.bmc.2007.09.046

upstream raw materials:

4-chloro-1,3-dimethyl-1H-pyrazolo[3,4-b]quinoline

4-methoxycarbonyl aniline

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