2-(trifluoromethyl)-N¹-(phenylsulfonyl)-N⁴-(bromoacetyl)benzoquinone diimine

Base Information

Chemical Name:2-(trifluoromethyl)-N¹-(phenylsulfonyl)-N⁴-(bromoacetyl)benzoquinone diimine
CAS No.:86785-31-1
Molecular Formula:C₁₅H₁₀BrF₃N₂O₃S
Molecular Weight:435.221
Hs Code.:

2-(trifluoromethyl)-N<sup>1</sup>-(phenylsulfonyl)-N<sup>4</sup>-(bromoacetyl)benzoquinone diimine

Synonyms:2-(trifluoromethyl)-N¹-(phenylsulfonyl)-N⁴-(bromoacetyl)benzoquinone diimine

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Chemical Property of 2-(trifluoromethyl)-N¹-(phenylsulfonyl)-N⁴-(bromoacetyl)benzoquinone diimine

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Technology Process of 2-(trifluoromethyl)-N¹-(phenylsulfonyl)-N⁴-(bromoacetyl)benzoquinone diimine

There total 6 articles about 2-(trifluoromethyl)-N¹-(phenylsulfonyl)-N⁴-(bromoacetyl)benzoquinone diimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 86785-42-4
2'-(trifluoromethyl)-4'-(bromoacetamido)benzenesulfonanilide

: 86785-31-1
2-(trifluoromethyl)-N¹-(phenylsulfonyl)-N⁴-(bromoacetyl)benzoquinone diimine

Guidance literature:: With lead(IV) acetate; In chloroform; for 2h; Ambient temperature;
DOI:10.1021/jo00167a002

Reference yield:

: 86802-68-8
N-(2-(trifluoromethyl)phenyl)benzenesulfonamide

: 86785-31-1
2-(trifluoromethyl)-N¹-(phenylsulfonyl)-N⁴-(bromoacetyl)benzoquinone diimine

Guidance literature:: Multi-step reaction with 4 steps

1: fuming nitric acid, aq. acetic acid / 24 h / steam bath

2: 60 percent / sodium dithionite / methanol; aq. NH₃ / 1.) 30 min, 2.) refrigerator, 1 h

3: 83 percent / sodium bromoacetate / acetonitrile / 24 h / Ambient temperature

4: 84 percent / lead tetraacetate / CHCl₃ / 2 h / Ambient temperature

With lead(IV) acetate; sodium dithionite; sodium 2-bromoacetate; nitric acid; acetic acid; In methanol; ammonium hydroxide; chloroform; acetonitrile;
DOI:10.1021/jo00167a002

Reference yield:

: 86785-37-7
2'-(trifluoromethyl)-4'-aminobenzenesulfonanilide

: 86785-31-1
2-(trifluoromethyl)-N¹-(phenylsulfonyl)-N⁴-(bromoacetyl)benzoquinone diimine

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / sodium bromoacetate / acetonitrile / 24 h / Ambient temperature

2: 84 percent / lead tetraacetate / CHCl₃ / 2 h / Ambient temperature

With lead(IV) acetate; sodium 2-bromoacetate; In chloroform; acetonitrile;
DOI:10.1021/jo00167a002