4-[4-((thiiran-2-yl)methylsulfonyl)phenoxy]benzamine hydrochloride salt

Base Information

Chemical Name:4-[4-((thiiran-2-yl)methylsulfonyl)phenoxy]benzamine hydrochloride salt
CAS No.:1333379-23-9
Molecular Formula:C₁₅H₁₅NO₃S₂*ClH
Molecular Weight:357.882
Hs Code.:

Synonyms:4-[4-((thiiran-2-yl)methylsulfonyl)phenoxy]benzamine hydrochloride salt

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Chemical Property of 4-[4-((thiiran-2-yl)methylsulfonyl)phenoxy]benzamine hydrochloride salt

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Technology Process of 4-[4-((thiiran-2-yl)methylsulfonyl)phenoxy]benzamine hydrochloride salt

There total 11 articles about 4-[4-((thiiran-2-yl)methylsulfonyl)phenoxy]benzamine hydrochloride salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.7%

: 1333379-22-8
tert-butyl (4-(4-((thiiran-2-ylmethyl)sulfonyl)phenoxy)phenyl)carbamate

: 1333379-23-9
4-[4-((thiiran-2-yl)methylsulfonyl)phenoxy]benzamine hydrochloride salt

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 20 ℃;
DOI:10.1016/j.bmc.2015.09.013

Reference yield:

: 1333481-74-5
tert-butyl (4-(4-((oxiran-2-ylmethyl)sulfonyl)phenoxy)phenyl)carbamate

: 1333379-23-9
4-[4-((thiiran-2-yl)methylsulfonyl)phenoxy]benzamine hydrochloride salt

Guidance literature:: Multi-step reaction with 2 steps

1: thiourea / methanol; dichloromethane / 18 h / 20 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane; dichloromethane; ethyl acetate / 48 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; thiourea; In 1,4-dioxane; methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm200566e

Reference yield:

: 1333379-21-7
t-butyl [4-(4-(allylthio)phenoxy)phenyl]carbamate

: 1333379-23-9
4-[4-((thiiran-2-yl)methylsulfonyl)phenoxy]benzamine hydrochloride salt

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 72 h / Inert atmosphere; Cooling with ice

2: thiourea / methanol; dichloromethane / 18 h / 20 °C / Inert atmosphere

3: hydrogenchloride / 1,4-dioxane; dichloromethane; ethyl acetate / 48 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; thiourea; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm200566e