1-Nitro-4-[(2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy]benzene

Base Information

Chemical Name:1-Nitro-4-[(2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy]benzene
CAS No.:183997-46-8
Molecular Formula:C₁₂H₆F₁₁NO₃
Molecular Weight:421.167
Hs Code.:
DSSTox Substance ID:DTXSID10896052
Nikkaji Number:J777.566K
Wikidata:Q82872266

Synonyms:1-Nitro-4-[(2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy]benzene;183997-46-8;DTXSID10896052;(4-Nitrophenyl)(2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl) ether

Suppliers and Price of 1-Nitro-4-[(2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy]benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Nitro-4-[(2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy]benzene

Chemical Property:

XLogP3:5.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:14
Rotatable Bond Count:6
Exact Mass:421.01720284
Heavy Atom Count:27
Complexity:536

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=CC=C1[N+](=O)[O-])OCC(C(C(C(C(F)(F)F)(F)F)(F)F)(F)F)(F)F

Technology Process of 1-Nitro-4-[(2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy]benzene

There total 3 articles about 1-Nitro-4-[(2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl)oxy]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 168632-11-9
2,2,3,3,4,4,5,5,6,6,6-undecafluorohexyl trifluoromethanesulfonate

: 183997-46-8
1-Nitro-4-(2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyloxy)-benzene

Guidance literature:: With sodium hydride; In N,N,N,N,N,N-hexamethylphosphoric triamide; 1.) r.t., 2.) 110 deg C, 8 h;
DOI:10.1016/S0022-1139(96)03490-2

Reference yield:

: 423-46-1
perfluorohexanol

: 183997-46-8
1-Nitro-4-(2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyloxy)-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / Et₃N / CH₂Cl₂ / 6 h / Ambient temperature

2: 98 percent / NaH / hexamethylphosphoric acid triamide / 1.) r.t., 2.) 110 deg C, 8 h

With sodium hydride; triethylamine; In N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1016/S0022-1139(96)03490-2

Reference yield:

: 307-24-4
undecafluorohexanoic acid

: 183997-46-8
1-Nitro-4-(2,2,3,3,4,4,5,5,6,6,6-undecafluoro-hexyloxy)-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: LAH

2: 62 percent / Et₃N / CH₂Cl₂ / 6 h / Ambient temperature

3: 98 percent / NaH / hexamethylphosphoric acid triamide / 1.) r.t., 2.) 110 deg C, 8 h

With lithium aluminium tetrahydride; sodium hydride; triethylamine; In N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1016/S0022-1139(96)03490-2