4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid

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Chemical Name:4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid
CAS No.:1314562-03-2
Molecular Formula:C₂₇H₁₈BrNO₅S
Molecular Weight:548.414
Hs Code.:

Synonyms:4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid

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Chemical Property of 4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid

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Technology Process of 4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid

There total 3 articles about 4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1314561-65-3
4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid methyl ester

: 1314562-03-2
4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid

Guidance literature:: With hydrogenchloride; water; acetic acid; for 4h; Reflux;
DOI:10.1016/j.ejmech.2011.05.012

Reference yield:

: 1314561-31-3
C₁₉H₁₂BrNO₃S

: 1314562-03-2
4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / toluene / 48 h / Reflux

2: hydrogenchloride; water; acetic acid / 4 h / Reflux

With hydrogenchloride; water; potassium carbonate; acetic acid; In toluene;
DOI:10.1016/j.ejmech.2011.05.012

Reference yield:

: (Z)-4-((2,4-dioxo-1,3-thiazolidin-5-ylidene)methyl)benzaldehyde

: 1314562-03-2
4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol

2: potassium carbonate / toluene / 48 h / Reflux

3: hydrogenchloride; water; acetic acid / 4 h / Reflux

With hydrogenchloride; water; potassium carbonate; acetic acid; potassium hydroxide; In ethanol; toluene; 1: Claisen-Schmidt condensation;
DOI:10.1016/j.ejmech.2011.05.012