4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid methyl ester

Base Information

Chemical Name:4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid methyl ester
CAS No.:1314561-65-3
Molecular Formula:C₂₈H₂₀BrNO₅S
Molecular Weight:562.441
Hs Code.:

Synonyms:4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid methyl ester

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Chemical Property of 4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid methyl ester

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Technology Process of 4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid methyl ester

There total 3 articles about 4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2417-72-3
Methyl 4-(bromomethyl)benzoate

: 1314561-31-3
C₁₉H₁₂BrNO₃S

: 1314561-65-3
4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid methyl ester

Guidance literature:: With potassium carbonate; In toluene; for 48h; Reflux;
DOI:10.1016/j.ejmech.2011.05.012

Reference yield:

: 623-27-8
terephthalaldehyde,

: 1314561-65-3
4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium acetate; acetic acid / Reflux

2: potassium hydroxide / ethanol

3: potassium carbonate / toluene / 48 h / Reflux

With sodium acetate; potassium carbonate; acetic acid; potassium hydroxide; In ethanol; toluene; 1: Knoevenagel condensation / 2: Claisen-Schmidt condensation;
DOI:10.1016/j.ejmech.2011.05.012

Reference yield:

: (Z)-4-((2,4-dioxo-1,3-thiazolidin-5-ylidene)methyl)benzaldehyde

: 1314561-65-3
4-(((Z)-5-(4-((E)-3-(2-bromophenyl)-3-oxoprop-1-en-1-yl)benzylidene)-2,4-dioxothiazolidin-3-yl)methyl)benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol

2: potassium carbonate / toluene / 48 h / Reflux

With potassium carbonate; potassium hydroxide; In ethanol; toluene; 1: Claisen-Schmidt condensation;
DOI:10.1016/j.ejmech.2011.05.012