C₄₀H₅₆N₄O₇S

Base Information

Chemical Name:C₄₀H₅₆N₄O₇S
CAS No.:1101181-34-3
Molecular Formula:C₄₀H₅₆N₄O₇S
Molecular Weight:736.973
Hs Code.:

C<sub>40</sub>H<sub>56</sub>N<sub>4</sub>O<sub>7</sub>S

Synonyms:C₄₀H₅₆N₄O₇S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₀H₅₆N₄O₇S

Chemical Property:

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Technology Process of C₄₀H₅₆N₄O₇S

There total 24 articles about C₄₀H₅₆N₄O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1017624-87-1
C₄₀H₅₄N₄O₇S

: 1101181-34-3
C₄₀H₅₆N₄O₇S

Guidance literature:: With dimethylsulfide borane complex; (S)-Corey-Bakshi-Shibata oxazaborolidine; In tetrahydrofuran; at 0 - 20 ℃; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jm8013579

Reference yield:

: 204917-42-0
(3S)-4-(tert-butyldimethylsilanyloxy)-3-methylbutyraldehyde

: 1101181-34-3
C₄₀H₅₆N₄O₇S

: C₄₀H₅₆N₄O₇S

Guidance literature:: Multi-step reaction with 11 steps

1: pyridinium p-toluenesulfonate; copper(II) sulfate / dichloromethane / 24 h

2: tetrahydrofuran / -78 - 20 °C

3: hydrogenchloride / 1,4-dioxane / 2 h / 0 °C

4: triethylamine / dichloromethane / 20 °C

5: dipyridinium dichromate / N,N-dimethyl-formamide / 24 h / 20 °C

6: lithium hydroxide monohydrate; dihydrogen peroxide / water; tetrahydrofuran / 20 °C

7: sodium hydrogencarbonate / dimethyl sulfoxide / 24 h

8: dichloromethane / 2 h / 0 °C

9: 1-hydroxy-7-aza-benzotriazole; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 15 h / 0 - 20 °C

10: hydrogenchloride / 1,4-dioxane / 2 h

11: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane

With hydrogenchloride; dipyridinium dichromate; 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; dihydrogen peroxide; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; copper(II) sulfate; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2016.08.038

Reference yield:

: 156592-93-7
(3S)-4-<(tert-butyldimethylsilyl)oxy>-3-methylbutanol

: 1101181-34-3
C₄₀H₅₆N₄O₇S

: C₄₀H₅₆N₄O₇S

Guidance literature:: Multi-step reaction with 12 steps

1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 3 h / -78 °C

2: pyridinium p-toluenesulfonate; copper(II) sulfate / dichloromethane / 24 h

3: tetrahydrofuran / -78 - 20 °C

4: hydrogenchloride / 1,4-dioxane / 2 h / 0 °C

5: triethylamine / dichloromethane / 20 °C

6: dipyridinium dichromate / N,N-dimethyl-formamide / 24 h / 20 °C

7: lithium hydroxide monohydrate; dihydrogen peroxide / water; tetrahydrofuran / 20 °C

8: sodium hydrogencarbonate / dimethyl sulfoxide / 24 h

9: dichloromethane / 2 h / 0 °C

10: 1-hydroxy-7-aza-benzotriazole; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 15 h / 0 - 20 °C

11: hydrogenchloride / 1,4-dioxane / 2 h

12: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane

With hydrogenchloride; dipyridinium dichromate; 1-hydroxy-7-aza-benzotriazole; oxalyl dichloride; lithium hydroxide monohydrate; dihydrogen peroxide; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; copper(II) sulfate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2016.08.038