6-O-(4-methoxytetrahydropyran-4-yl)-1,2:4,5-di-O-isopropylidene-D-myo-inositol

Base Information

Chemical Name:6-O-(4-methoxytetrahydropyran-4-yl)-1,2:4,5-di-O-isopropylidene-D-myo-inositol
CAS No.:124649-44-1
Molecular Formula:C₁₈H₃₀O₈
Molecular Weight:374.431
Hs Code.:

Synonyms:6-O-(4-methoxytetrahydropyran-4-yl)-1,2:4,5-di-O-isopropylidene-D-myo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-O-(4-methoxytetrahydropyran-4-yl)-1,2:4,5-di-O-isopropylidene-D-myo-inositol

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Technology Process of 6-O-(4-methoxytetrahydropyran-4-yl)-1,2:4,5-di-O-isopropylidene-D-myo-inositol

There total 5 articles about 6-O-(4-methoxytetrahydropyran-4-yl)-1,2:4,5-di-O-isopropylidene-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 119874-37-2,124648-23-3
3-O-(tert-butyldiphenylsilyl)-6-O-(4-methoxytetrahydropyran-4-yl)-1,2:4,5-di-O-isopropylidene-D-myo-inositol

: 124649-44-1
6-O-(4-methoxytetrahydropyran-4-yl)-1,2:4,5-di-O-isopropylidene-D-myo-inositol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 16h; Ambient temperature;
DOI:10.1021/jm00164a027

Reference yield:

: 119874-35-0,119943-93-0,124648-22-2
1⁽³⁾-O-(tert-butyldiphenylsilyl)-2,3⁽¹⁾:5,6⁽⁴⁾-di-O-isopropylidene-D-myo-inositol

: 124649-44-1
6-O-(4-methoxytetrahydropyran-4-yl)-1,2:4,5-di-O-isopropylidene-D-myo-inositol

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dioxane / Ambient temperature; overnight

2: 93 percent / KOH / ethanol / 0.5 h / Ambient temperature

3: 96 percent / pyridinium p-toluenesulfonate, 4-Angstroem molecular sieves / CH₂Cl₂ / Ambient temperature; overnight

4: 55 percent / tetrabutylammonium fluoride / tetrahydrofuran / 16 h / Ambient temperature

With pyridine; potassium hydroxide; 4 A molecular sieve; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane;
DOI:10.1021/jm00164a027

Reference yield:

: 17327-22-9
4-methoxy-2,6-dihydropyran

: 124649-44-1
6-O-(4-methoxytetrahydropyran-4-yl)-1,2:4,5-di-O-isopropylidene-D-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / pyridinium p-toluenesulfonate, 4-Angstroem molecular sieves / CH₂Cl₂ / Ambient temperature; overnight

2: 55 percent / tetrabutylammonium fluoride / tetrahydrofuran / 16 h / Ambient temperature

With 4 A molecular sieve; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00164a027