ethyl (4E)-8-benzyloxy-4-enoctanoate

Base Information Edit

Chemical Name:ethyl (4E)-8-benzyloxy-4-enoctanoate
CAS No.:181803-05-4
Molecular Formula:C₁₇H₂₄O₃
Molecular Weight:276.376
Hs Code.:
Mol file:181803-05-4.mol

Synonyms:ethyl (4E)-8-benzyloxy-4-enoctanoate

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Chemical Property of ethyl (4E)-8-benzyloxy-4-enoctanoate Edit

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Technology Process of ethyl (4E)-8-benzyloxy-4-enoctanoate

There total 2 articles about ethyl (4E)-8-benzyloxy-4-enoctanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 126260-80-8
(3RS)-6-benzyloxyhex-1-en-3-ol

: 78-39-7
Triethyl orthoacetate

: 181803-05-4
ethyl (4E)-8-benzyloxy-4-enoctanoate

Guidance literature:: With propionic acid; at 140 ℃; for 3h; Inert atmosphere;
DOI:10.1055/s-0029-1216928

Reference yield:

: 5470-84-8
4-benzyloxybutanal

: 181803-05-4
ethyl (4E)-8-benzyloxy-4-enoctanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / tetrahydrofuran / 5 h / 0 °C

2: propionic acid / xylene / 2.5 h / Heating

With propionic acid; In tetrahydrofuran; xylene; 1: Grignard reaction / 2: Claisen-Johnson rearrangement;
DOI:10.1021/jo000500a