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Technology Process of B10C2H10CH3(CH2(C6H4)C2H)

B10C2H10CH3(CH2(C6H4)C2H)

Base Information
  • Chemical Name:B10C2H10CH3(CH2(C6H4)C2H)
  • CAS No.:1174636-38-4
  • Molecular Formula:C12H20B10
  • Molecular Weight:272.401
  • Hs Code.:
B<sub>10</sub>C<sub>2</sub>H<sub>10</sub>CH<sub>3</sub>(CH<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>)C<sub>2</sub>H)

Synonyms:B10C2H10CH3(CH2(C6H4)C2H)

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Chemical Property of B10C2H10CH3(CH2(C6H4)C2H)
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Technology Process of B10C2H10CH3(CH2(C6H4)C2H)

There total 1 articles about B10C2H10CH3(CH2(C6H4)C2H) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

B<sub>10</sub>C<sub>2</sub>H<sub>10</sub>CH<sub>3</sub>(CH<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>)C<sub>2</sub>TMS)
1174636-37-3

B10C2H10CH3(CH2(C6H4)C2TMS)

B<sub>10</sub>C<sub>2</sub>H<sub>10</sub>CH<sub>3</sub>(CH<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>)C<sub>2</sub>H)
1174636-38-4

B10C2H10CH3(CH2(C6H4)C2H)

Guidance literature:
With K2CO3; In tetrahydrofuran; methanol; K2CO3 was added to soln. of carborane in THF/MeOH (1:1, v/v), stirred atroom temp. for 5 h; filtered through cotton, evapd., column chromy. (silica, 20% EtOAc in hexane), elem. anal.;
DOI:10.1021/ic101729s

Reference yield: 92.0%

B<sub>10</sub>C<sub>2</sub>H<sub>10</sub>CH<sub>3</sub>(CH<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>)C<sub>2</sub>H)
1174636-38-4

B10C2H10CH3(CH2(C6H4)C2H)

p-xylylene diazide
102437-81-0

p-xylylene diazide

C<sub>20</sub>H<sub>28</sub>B<sub>10</sub>N<sub>6</sub>

C20H28B10N6

Guidance literature:
With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; at 20 ℃; Inert atmosphere;
DOI:10.1021/ic4013697

Reference yield: 66.0%

B<sub>10</sub>C<sub>2</sub>H<sub>10</sub>CH<sub>3</sub>(CH<sub>2</sub>(C<sub>6</sub>H<sub>4</sub>)C<sub>2</sub>H)
1174636-38-4

B10C2H10CH3(CH2(C6H4)C2H)

1-(azidomethyl)-4-vinylbenzene
111965-73-2

1-(azidomethyl)-4-vinylbenzene

(B<sub>10</sub>C<sub>2</sub>H<sub>10</sub>(CH<sub>3</sub>)(CH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>CCHN<sub>3</sub>CH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>))CHCH<sub>2</sub>

(B10C2H10(CH3)(CH2C6H4CCHN3CH2C6H4))CHCH2

Guidance literature:
With CuSO4; sodium ascorbate; In tetrahydrofuran; water; polystyrene polymer and carborane deriv. dissolved in THF, aq. CuSO4 added, then aq. Na ascorbate added dropwise, stirred at 25°C overnight; THF removed under vac., CH2Cl2 and aq. ammonia added, stirred for 1 h; org. phase washed 3 times with water, dried with Na2SO4, solvent removed under vac., pptd. twice with CH2Cl2/MeOH;
DOI:10.1002/ejic.201100360
upstream raw materials:

B10C2H10CH3(CH2(C6H4)C2TMS)

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