(1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)trifluoroborane

Base Information

Chemical Name:(1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)trifluoroborane
CAS No.:797056-39-4
Molecular Formula:C₂₁H₂₄BF₃N₂
Molecular Weight:372.241
Hs Code.:

Synonyms:(1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)trifluoroborane

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Chemical Property of (1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)trifluoroborane

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Technology Process of (1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)trifluoroborane

There total 3 articles about (1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)trifluoroborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 141556-42-5
[1,3-bis(2,4,6-trimethylphenyl)imidazol]-2-ylidene

: 797056-39-4
(1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)trifluoroborane

Guidance literature:: With boron trifluoride diethyl etherate; In tetrahydrofuran; at 20 ℃; for 0.5h;

Reference yield: 55.0%

: 797056-36-1
(1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)triethylborane

: 109-63-7
trifluoroborane diethyl ether

: 797056-39-4
(1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)trifluoroborane

Guidance literature:: In dichloromethane; a soln. of ylidene compd. treated at -78°C with borane, warmed toroom temp.; elem. anal., IR, NMR;
DOI:10.1039/b405459h

Reference yield:

: 141556-45-8
1,3-bis(mesityl)imidazolium chloride

: 797056-39-4
(1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)trifluoroborane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: dichloromethane

In tetrahydrofuran; dichloromethane;
DOI:10.1039/b405459h