N-dodecyl-[N^α-(benzyloxycarbonyl)-N^ε-(tert-butyloxycarbonyl)]lysinamide

Base Information

Chemical Name:N-dodecyl-[N^α-(benzyloxycarbonyl)-N^ε-(tert-butyloxycarbonyl)]lysinamide
CAS No.:888616-04-4
Molecular Formula:C₃₁H₅₃N₃O₅
Molecular Weight:547.779
Hs Code.:

N-dodecyl-[N<sup>α</sup>-(benzyloxycarbonyl)-N<sup>ε</sup>-(tert-butyloxycarbonyl)]lysinamide

Synonyms:N-dodecyl-[N^α-(benzyloxycarbonyl)-N^ε-(tert-butyloxycarbonyl)]lysinamide

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Chemical Property of N-dodecyl-[N^α-(benzyloxycarbonyl)-N^ε-(tert-butyloxycarbonyl)]lysinamide

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Technology Process of N-dodecyl-[N^α-(benzyloxycarbonyl)-N^ε-(tert-butyloxycarbonyl)]lysinamide

There total 1 articles about N-dodecyl-[N^α-(benzyloxycarbonyl)-N^ε-(tert-butyloxycarbonyl)]lysinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 124-22-1
n-Dodecylamine

: 2389-60-8
Z-Lys(Boc)-OH

: 888616-04-4
N-dodecyl-[N^α-(benzyloxycarbonyl)-N^ε-(tert-butyloxycarbonyl)]lysinamide

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1039/b513944a

Reference yield:

: 888616-04-4
N-dodecyl-[N^α-(benzyloxycarbonyl)-N^ε-(tert-butyloxycarbonyl)]lysinamide

: 888616-05-5
N-[1-(dodecylcarbamoyl)-4-(tert-butyloxycarbonylamino)butyl]-22-(benzyloxycarbonylamino)-12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19-hexadecafluorodocosanamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / Pd/C / ethanol / 6 h / 20 °C / 6000.48 Torr

2: 415.3 mg / diisopropylethylamine; TBTU / CH₂Cl₂ / 12 h / 20 °C / pH 8

With hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1039/b513944a