Dithiocarbonic acid O-[(2S,3S,5R,6R)-5-(4-bromo-benzyloxy)-2-[1,3]dioxolan-2-ylmethyl-6-methoxymethyl-tetrahydro-pyran-3-yl] ester S-methyl ester

Base Information

• Chemical Name: Dithiocarbonic acid O-[(2S,3S,5R,6R)-5-(4-bromo-benzyloxy)-2-[1,3]dioxolan-2-ylmethyl-6-methoxymethyl-tetrahydro-pyran-3-yl] ester S-methyl ester
• CAS No.: 120005-53-0
• Molecular Formula: C₂₀H₂₇BrO₆S₂
• Molecular Weight: 507.467

Synonyms:Dithiocarbonic acid O-[(2S,3S,5R,6R)-5-(4-bromo-benzyloxy)-2-[1,3]dioxolan-2-ylmethyl-6-methoxymethyl-tetrahydro-pyran-3-yl] ester S-methyl ester

Chemical Property of Dithiocarbonic acid O-[(2S,3S,5R,6R)-5-(4-bromo-benzyloxy)-2-[1,3]dioxolan-2-ylmethyl-6-methoxymethyl-tetrahydro-pyran-3-yl] ester S-methyl ester

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Technology Process of Dithiocarbonic acid O-[(2S,3S,5R,6R)-5-(4-bromo-benzyloxy)-2-[1,3]dioxolan-2-ylmethyl-6-methoxymethyl-tetrahydro-pyran-3-yl] ester S-methyl ester

There total 1 articles about Dithiocarbonic acid O-[(2S,3S,5R,6R)-5-(4-bromo-benzyloxy)-2-[1,3]dioxolan-2-ylmethyl-6-methoxymethyl-tetrahydro-pyran-3-yl] ester S-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

carbon disulfide (75-15-0,12122-00-8) + (2S,3S,5R,6R)-5-(4-Bromo-benzyloxy)-2-[1,3]dioxolan-2-ylmethyl-6-methoxymethyl-tetrahydro-pyran-3-ol (120005-52-9) + methyl iodide (74-88-4) → Dithiocarbonic acid O-[(2S,3S,5R,6R)-5-(4-bromo-benzyloxy)-2-[1,3]dioxolan-2-ylmethyl-6-methoxymethyl-tetrahydro-pyran-3-yl] ester S-methyl ester (120005-53-0)

Guidance literature:

With sodium hydride;

DOI:10.1016/0040-4039(88)85083-4

Reference yield: 91.0%

Dithiocarbonic acid O-[(2S,3S,5R,6R)-5-(4-bromo-benzyloxy)-2-[1,3]dioxolan-2-ylmethyl-6-methoxymethyl-tetrahydro-pyran-3-yl] ester S-methyl ester (120005-53-0) → (2R,3R,5S,6S)-3-(4-Bromo-benzyloxy)-5-chloro-6-[1,3]dioxolan-2-ylmethyl-2-methoxymethyl-tetrahydro-pyran (120005-54-1)

Guidance literature:

With sulfuryl dichloride; In chloroform;

DOI:10.1021/jo00290a014

upstream raw materials:

carbon disulfide

(2S,3S,5R,6R)-5-(4-Bromo-benzyloxy)-2-[1,3]dioxolan-2-ylmethyl-6-methoxymethyl-tetrahydro-pyran-3-ol

methyl iodide

Downstream raw materials:

(2R,3R,5S,6S)-3-(4-Bromo-benzyloxy)-5-chloro-6-[1,3]dioxolan-2-ylmethyl-2-methoxymethyl-tetrahydro-pyran

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