(R)-tert-butyl (1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethyl)carbamate

Base Information

Chemical Name:(R)-tert-butyl (1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethyl)carbamate
CAS No.:1415728-60-7
Molecular Formula:C₁₆H₁₉Cl₂N₃O₂
Molecular Weight:356.252
Hs Code.:

Synonyms:(R)-tert-butyl (1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethyl)carbamate

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Chemical Property of (R)-tert-butyl (1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethyl)carbamate

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Technology Process of (R)-tert-butyl (1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethyl)carbamate

There total 5 articles about (R)-tert-butyl (1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4248-19-5
tert-butyl carbazate

: 1415728-60-7
(R)-tert-butyl (1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: formic acid / methanol; water / 72 h / 20 °C

2: potassium carbonate; sodium sulfate / tetrahydrofuran / 5 h / Reflux

3: (1R,2R)-N¹,N²-bis[4-(1-pyrrolidinyl)-2-quinolinyl]-1,2-cyclohexanediamine / toluene / 48 h / -78 - -20 °C

4: cobalt(II) chloride; sodium tetrahydroborate / methanol / 0 - 20 °C

5: ammonium acetate / methanol; water / 20 h / Reflux

With sodium tetrahydroborate; formic acid; (1R,2R)-N¹,N²-bis[4-(1-pyrrolidinyl)-2-quinolinyl]-1,2-cyclohexanediamine; ammonium acetate; potassium carbonate; sodium sulfate; cobalt(II) chloride; In tetrahydrofuran; methanol; water; toluene;
DOI:10.1021/ol303092v

Reference yield:

: 163226-26-4
tert-butyl 2,4-dichlorobenzylidenecarbamate

: 1415728-60-7
(R)-tert-butyl (1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: (1R,2R)-N¹,N²-bis[4-(1-pyrrolidinyl)-2-quinolinyl]-1,2-cyclohexanediamine / toluene / 48 h / -78 - -20 °C

2: cobalt(II) chloride; sodium tetrahydroborate / methanol / 0 - 20 °C

3: ammonium acetate / methanol; water / 20 h / Reflux

With sodium tetrahydroborate; (1R,2R)-N¹,N²-bis[4-(1-pyrrolidinyl)-2-quinolinyl]-1,2-cyclohexanediamine; ammonium acetate; cobalt(II) chloride; In methanol; water; toluene;
DOI:10.1021/ol303092v

Reference yield:

: tert-butyl ((1R)-2-bromo-1-(2,4-dichlorophenyl)-2-nitroethyl)carbamate

: 1415728-60-7
(R)-tert-butyl (1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: cobalt(II) chloride; sodium tetrahydroborate / methanol / 0 - 20 °C

2: ammonium acetate / methanol; water / 20 h / Reflux

With sodium tetrahydroborate; ammonium acetate; cobalt(II) chloride; In methanol; water;
DOI:10.1021/ol303092v