dimethyl 2-(allyl(2-(2-((E)-5-methoxy-5-oxopent-1-enyl)-1-tosyl-1H-indol-3-yl)ethyl)amino)maleate

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Chemical Name:dimethyl 2-(allyl(2-(2-((E)-5-methoxy-5-oxopent-1-enyl)-1-tosyl-1H-indol-3-yl)ethyl)amino)maleate
CAS No.:1397694-08-4
Molecular Formula:C₃₂H₃₆N₂O₈S
Molecular Weight:608.712
Hs Code.:

Synonyms:dimethyl 2-(allyl(2-(2-((E)-5-methoxy-5-oxopent-1-enyl)-1-tosyl-1H-indol-3-yl)ethyl)amino)maleate

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Chemical Property of dimethyl 2-(allyl(2-(2-((E)-5-methoxy-5-oxopent-1-enyl)-1-tosyl-1H-indol-3-yl)ethyl)amino)maleate

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Technology Process of dimethyl 2-(allyl(2-(2-((E)-5-methoxy-5-oxopent-1-enyl)-1-tosyl-1H-indol-3-yl)ethyl)amino)maleate

There total 2 articles about dimethyl 2-(allyl(2-(2-((E)-5-methoxy-5-oxopent-1-enyl)-1-tosyl-1H-indol-3-yl)ethyl)amino)maleate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1397693-93-4
dimethyl 2-(allyl(2-(2-((E)-6-methoxy-4-(methoxycarbonyl)-5,6-dioxohex-1-enyl)-1-tosyl-1H-indol-3-yl)ethyl)amino)maleate

: 1397694-08-4
dimethyl 2-(allyl(2-(2-((E)-5-methoxy-5-oxopent-1-enyl)-1-tosyl-1H-indol-3-yl)ethyl)amino)maleate

Guidance literature:: With sodium hydroxide; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1039/c2ob25755f

Reference yield:

: 1068441-76-8
2-allyl-9-tosyl-1-vinyl-2,3,4,9-tetrahydro-1H-β-carboline

: 1397694-08-4
dimethyl 2-(allyl(2-(2-((E)-5-methoxy-5-oxopent-1-enyl)-1-tosyl-1H-indol-3-yl)ethyl)amino)maleate

Guidance literature:: Multi-step reaction with 2 steps

1: gold(III) chloride / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

2: sodium hydroxide / dichloromethane / 20 °C / Inert atmosphere

With gold(III) chloride; sodium hydroxide; In dichloromethane;
DOI:10.1039/c2ob25755f