(4-((4-methoxyphenethyl)carbamoyl)phenyl)diphenylsulfonium trifluoromethanesulfonate

Base Information

Chemical Name:(4-((4-methoxyphenethyl)carbamoyl)phenyl)diphenylsulfonium trifluoromethanesulfonate
CAS No.:1374560-88-9
Molecular Formula:CF₃O₃S*C₂₈H₂₆NO₂S
Molecular Weight:589.656
Hs Code.:

Synonyms:(4-((4-methoxyphenethyl)carbamoyl)phenyl)diphenylsulfonium trifluoromethanesulfonate

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Chemical Property of (4-((4-methoxyphenethyl)carbamoyl)phenyl)diphenylsulfonium trifluoromethanesulfonate

Chemical Property:

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Technology Process of (4-((4-methoxyphenethyl)carbamoyl)phenyl)diphenylsulfonium trifluoromethanesulfonate

There total 3 articles about (4-((4-methoxyphenethyl)carbamoyl)phenyl)diphenylsulfonium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1229186-21-3
(4-carboxyphenyl)(diphenyl)sulfonium trifluoromethanesulfonate

: 55-81-2
4-Methoxyphenethylamine

: 1374560-88-9
(4-((4-methoxyphenethyl)carbamoyl)phenyl)diphenylsulfonium trifluoromethanesulfonate

Guidance literature:: (4-carboxyphenyl)(diphenyl)sulfonium trifluoromethanesulfonate; With 4-methyl-morpholine; 4‐(4,6dimethoxy‐1,3,5‐triazin‐2‐yl)‐4‐methylmorpholinium tetrafluoroborate; In N,N-dimethyl-formamide; at 20 ℃; for 0.666667h;

4-Methoxyphenethylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1002/ejoc.201101730

Reference yield:

: 945-51-7
1,1'-sulfinylbisbenzene

: 1374560-88-9
(4-((4-methoxyphenethyl)carbamoyl)phenyl)diphenylsulfonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.17 h / 20 °C

1.2: 3.5 h / -40 - -10 °C

2.1: 4-methyl-morpholine; 4‐(4,6dimethoxy‐1,3,5‐triazin‐2‐yl)‐4‐methylmorpholinium tetrafluoroborate / N,N-dimethyl-formamide / 0.67 h / 20 °C

2.2: 20 °C

With 4-methyl-morpholine; 4‐(4,6dimethoxy‐1,3,5‐triazin‐2‐yl)‐4‐methylmorpholinium tetrafluoroborate; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201101730

Reference yield:

: 619-58-9
4-iodobenzoic acid

: 1374560-88-9
(4-((4-methoxyphenethyl)carbamoyl)phenyl)diphenylsulfonium trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.17 h / 20 °C

1.2: 3.5 h / -40 - -10 °C

2.1: 4-methyl-morpholine; 4‐(4,6dimethoxy‐1,3,5‐triazin‐2‐yl)‐4‐methylmorpholinium tetrafluoroborate / N,N-dimethyl-formamide / 0.67 h / 20 °C

2.2: 20 °C

With 4-methyl-morpholine; 4‐(4,6dimethoxy‐1,3,5‐triazin‐2‐yl)‐4‐methylmorpholinium tetrafluoroborate; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201101730