7-(3,5-dimethylisoxazol-4-yl)-8-methoxy-1-((R)-1-phenylethyl)-1H-imidazo[4,5-c]quinoline-2(3H)-thione

Base Information

Chemical Name:7-(3,5-dimethylisoxazol-4-yl)-8-methoxy-1-((R)-1-phenylethyl)-1H-imidazo[4,5-c]quinoline-2(3H)-thione
CAS No.:1300736-25-7
Molecular Formula:C₂₄H₂₂N₄O₂S
Molecular Weight:430.53
Hs Code.:

Synonyms:7-(3,5-dimethylisoxazol-4-yl)-8-methoxy-1-((R)-1-phenylethyl)-1H-imidazo[4,5-c]quinoline-2(3H)-thione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(3,5-dimethylisoxazol-4-yl)-8-methoxy-1-((R)-1-phenylethyl)-1H-imidazo[4,5-c]quinoline-2(3H)-thione

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 7-(3,5-dimethylisoxazol-4-yl)-8-methoxy-1-((R)-1-phenylethyl)-1H-imidazo[4,5-c]quinoline-2(3H)-thione

There total 10 articles about 7-(3,5-dimethylisoxazol-4-yl)-8-methoxy-1-((R)-1-phenylethyl)-1H-imidazo[4,5-c]quinoline-2(3H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1300031-63-3
7-(3,5-dimethylisoxazol-4-yl)-6-methoxy-N⁴-((R)-1-phenylethyl)quinoline-3,4-diamine

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 1300736-25-7
7-(3,5-dimethylisoxazol-4-yl)-8-methoxy-1-((R)-1-phenylethyl)-1H-imidazo[4,5-c]quinoline-2(3H)-thione

Guidance literature:: With pyridine; In tetrahydrofuran; at 80 ℃; for 1h;

Reference yield:

: 1300031-64-4
7-(3,5-dimethylisoxazol-4-yl)-6-methoxy-3-nitro-N-((R)-1-phenylethyl)quinolin-4-amine

: 1300736-25-7
7-(3,5-dimethylisoxazol-4-yl)-8-methoxy-1-((R)-1-phenylethyl)-1H-imidazo[4,5-c]quinoline-2(3H)-thione

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; tin(II) chloride dihdyrate / ethanol / 1 h / 40 °C

2: pyridine / tetrahydrofuran / 1 h / 80 °C

With pyridine; hydrogenchloride; tin(II) chloride dihdyrate; In tetrahydrofuran; ethanol;

Reference yield:

: 5-((3-(3,5-dimethylisoxazol-4-yl)-4-methoxyphenylamino)methylene)-2,2-dimethyl-1,3-dioxane-4,6-dione

: 1300736-25-7
7-(3,5-dimethylisoxazol-4-yl)-8-methoxy-1-((R)-1-phenylethyl)-1H-imidazo[4,5-c]quinoline-2(3H)-thione

Guidance literature:: Multi-step reaction with 6 steps

1: diphenylether / 0.5 h / 260 °C

2: nitric acid; propionic acid / 1 h / 125 °C

3: trichlorophosphate / 2 h / Reflux

4: 1 h / 70 °C

5: hydrogenchloride; tin(II) chloride dihdyrate / ethanol / 1 h / 40 °C

6: pyridine / tetrahydrofuran / 1 h / 80 °C

With pyridine; hydrogenchloride; tin(II) chloride dihdyrate; nitric acid; propionic acid; trichlorophosphate; In tetrahydrofuran; diphenylether; ethanol;