R-2-[N₁-(N₄-benzyloxycarbonylcytosinyl)-acetylamino]-3-tert-butyloxycarbonylamino-1-propanol

Base Information

• Chemical Name: R-2-[N₁-(N₄-benzyloxycarbonylcytosinyl)-acetylamino]-3-tert-butyloxycarbonylamino-1-propanol
• CAS No.: 1246279-60-6
• Molecular Formula: C₂₂H₂₉N₅O₇
• Molecular Weight: 475.502

Synonyms:R-2-[N₁-(N₄-benzyloxycarbonylcytosinyl)-acetylamino]-3-tert-butyloxycarbonylamino-1-propanol

Chemical Property of R-2-[N₁-(N₄-benzyloxycarbonylcytosinyl)-acetylamino]-3-tert-butyloxycarbonylamino-1-propanol

Chemical Property:

Purity/Quality:

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Technology Process of R-2-[N₁-(N₄-benzyloxycarbonylcytosinyl)-acetylamino]-3-tert-butyloxycarbonylamino-1-propanol

There total 1 articles about R-2-[N₁-(N₄-benzyloxycarbonylcytosinyl)-acetylamino]-3-tert-butyloxycarbonylamino-1-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

R-1-O-tert-butyldimethylsilyl-2-[N1-(N4-benzyloxycarbonylcytosinyl)-acetylamino]-3-tert-butyloxycarbonylamino-1-propanol (1246279-55-9) → R-2-[N1-(N4-benzyloxycarbonylcytosinyl)-acetylamino]-3-tert-butyloxycarbonylamino-1-propanol (1246279-60-6)

Guidance literature:

With iodine; In methanol;

DOI:10.1039/c003405n

Reference yield: 70.0%

R-2-[N1-(N4-benzyloxycarbonylcytosinyl)-acetylamino]-3-tert-butyloxycarbonylamino-1-propanol (1246279-60-6) + 4-Nitrophenyl chloroformate (7693-46-1) → R-1-O-p-nitrophenoxycarbonyl-2-[N1-(N4-benzyloxycarbonylcytosinyl)-acetylamino]-3-tert-butyloxycarbonylamino-1-propanol (1246279-65-1)

Guidance literature:

R-2-[N₁-(N₄-benzyloxycarbonylcytosinyl)-acetylamino]-3-tert-butyloxycarbonylamino-1-propanol; With pyridine; In dichloromethane; at 0 ℃;

4-Nitrophenyl chloroformate; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1039/c003405n

upstream raw materials:

R-1-O-tert-butyldimethylsilyl-2-[N₁-(N₄-benzyloxycarbonylcytosinyl)-acetylamino]-3-tert-butyloxycarbonylamino-1-propanol

Downstream raw materials:

R-1-O-p-nitrophenoxycarbonyl-2-[N₁-(N₄-benzyloxycarbonylcytosinyl)-acetylamino]-3-tert-butyloxycarbonylamino-1-propanol

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