8-(3-oxo-3-p-tolylprop-1-enyl)-3,4-dihydro-2H,6H-3,6-epoxy-naphtho[2,1-b] [1,5]dioxocine

Base Information

Chemical Name:8-(3-oxo-3-p-tolylprop-1-enyl)-3,4-dihydro-2H,6H-3,6-epoxy-naphtho[2,1-b] [1,5]dioxocine
CAS No.:1342894-93-2
Molecular Formula:C₂₄H₂₀O₄
Molecular Weight:372.42
Hs Code.:

Synonyms:8-(3-oxo-3-p-tolylprop-1-enyl)-3,4-dihydro-2H,6H-3,6-epoxy-naphtho[2,1-b] [1,5]dioxocine

Suppliers and Price of 8-(3-oxo-3-p-tolylprop-1-enyl)-3,4-dihydro-2H,6H-3,6-epoxy-naphtho[2,1-b] [1,5]dioxocine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 8-(3-oxo-3-p-tolylprop-1-enyl)-3,4-dihydro-2H,6H-3,6-epoxy-naphtho[2,1-b] [1,5]dioxocine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 8-(3-oxo-3-p-tolylprop-1-enyl)-3,4-dihydro-2H,6H-3,6-epoxy-naphtho[2,1-b] [1,5]dioxocine

There total 3 articles about 8-(3-oxo-3-p-tolylprop-1-enyl)-3,4-dihydro-2H,6H-3,6-epoxy-naphtho[2,1-b] [1,5]dioxocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(E)-1-hydroxy-4-(3-oxo-3-p-tolylprop-1-enyl)-2-naphthaldehyde: 1287259-42-0
(E)-1-hydroxy-4-(3-oxo-3-p-tolylprop-1-enyl)-2-naphthaldehyde

: 106-89-8,24969-06-0,13403-37-7
epichlorohydrin

: 1342894-93-2
8-(3-oxo-3-p-tolylprop-1-enyl)-3,4-dihydro-2H,6H-3,6-epoxy-naphtho[2,1-b] [1,5]dioxocine

Guidance literature:: With triethylamine; Reflux;
DOI:10.1016/j.bmcl.2012.01.009

Reference yield:

: 90-15-3
α-naphthol

: 1342894-93-2
8-(3-oxo-3-p-tolylprop-1-enyl)-3,4-dihydro-2H,6H-3,6-epoxy-naphtho[2,1-b] [1,5]dioxocine

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / 3 h / 120 °C

1.2: 2 h / 90 - 100 °C

2.1: hydrogenchloride / 1,4-dioxane / 80 - 90 °C

3.1: triethylamine / Reflux

With hydrogenchloride; triethylamine; trifluoroacetic acid; In 1,4-dioxane; 1.1: Duff reaction / 1.2: Duff reaction;
DOI:10.1016/j.bmcl.2012.01.009

Reference yield:

4-hydroxy-naphthalene-1,3-dicarbaldehyde: 4-hydroxy-naphthalene-1,3-dicarbaldehyde

: 122-00-9
para-methylacetophenone

: 1342894-93-2
8-(3-oxo-3-p-tolylprop-1-enyl)-3,4-dihydro-2H,6H-3,6-epoxy-naphtho[2,1-b] [1,5]dioxocine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane / 80 - 90 °C

2: triethylamine / Reflux

With hydrogenchloride; triethylamine; In 1,4-dioxane;
DOI:10.1016/j.bmcl.2012.01.009