4-methylamino-3-nitro-benzoic acid-N-phenyl-N-(2-ethoxycarbonylethyl)amide

Base Information

Chemical Name:4-methylamino-3-nitro-benzoic acid-N-phenyl-N-(2-ethoxycarbonylethyl)amide
CAS No.:211915-71-8
Molecular Formula:C₁₉H₂₁N₃O₅
Molecular Weight:371.393
Hs Code.:

Synonyms:4-methylamino-3-nitro-benzoic acid-N-phenyl-N-(2-ethoxycarbonylethyl)amide

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Chemical Property of 4-methylamino-3-nitro-benzoic acid-N-phenyl-N-(2-ethoxycarbonylethyl)amide

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Technology Process of 4-methylamino-3-nitro-benzoic acid-N-phenyl-N-(2-ethoxycarbonylethyl)amide

There total 4 articles about 4-methylamino-3-nitro-benzoic acid-N-phenyl-N-(2-ethoxycarbonylethyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 62750-11-2
ethyl 3-phenylaminopropionate

: 82357-48-0
4-methylamino-3-nitro-benzoic acid chloride

: 211915-71-8
4-methylamino-3-nitro-benzoic acid-N-phenyl-N-(2-ethoxycarbonylethyl)amide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h; Reagent/catalyst; Solvent;

Reference yield:

: 41263-74-5
4-(methylamino)-3-nitrobenzoic acid

: 211915-71-8
4-methylamino-3-nitro-benzoic acid-N-phenyl-N-(2-ethoxycarbonylethyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / dimethylformamide / 0.5 h / Heating

2: Et₃N / tetrahydrofuran / 20 °C

With thionyl chloride; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm0109513

Reference yield:

: 62-53-3
aniline

: 211915-71-8
4-methylamino-3-nitro-benzoic acid-N-phenyl-N-(2-ethoxycarbonylethyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethanol / 24 h / 100 °C / Inert atmosphere

2: triethylamine / dichloromethane / 12 h / 20 °C

With triethylamine; In ethanol; dichloromethane;