N-methyl-2-(4-(4-methyl-6-((tetrahydro-2H-pyran-2-yl)oxy)-3-(3-((tetrahydro-2H-pyran-2-yl)oxy)phenyl)-2H-chromen-2-yl)phenoxy)ethanamine

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Chemical Name:N-methyl-2-(4-(4-methyl-6-((tetrahydro-2H-pyran-2-yl)oxy)-3-(3-((tetrahydro-2H-pyran-2-yl)oxy)phenyl)-2H-chromen-2-yl)phenoxy)ethanamine
CAS No.:1352306-74-1
Molecular Formula:C₃₅H₄₁NO₆
Molecular Weight:571.714
Hs Code.:

Synonyms:N-methyl-2-(4-(4-methyl-6-((tetrahydro-2H-pyran-2-yl)oxy)-3-(3-((tetrahydro-2H-pyran-2-yl)oxy)phenyl)-2H-chromen-2-yl)phenoxy)ethanamine

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Chemical Property of N-methyl-2-(4-(4-methyl-6-((tetrahydro-2H-pyran-2-yl)oxy)-3-(3-((tetrahydro-2H-pyran-2-yl)oxy)phenyl)-2H-chromen-2-yl)phenoxy)ethanamine

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Technology Process of N-methyl-2-(4-(4-methyl-6-((tetrahydro-2H-pyran-2-yl)oxy)-3-(3-((tetrahydro-2H-pyran-2-yl)oxy)phenyl)-2H-chromen-2-yl)phenoxy)ethanamine

There total 9 articles about N-methyl-2-(4-(4-methyl-6-((tetrahydro-2H-pyran-2-yl)oxy)-3-(3-((tetrahydro-2H-pyran-2-yl)oxy)phenyl)-2H-chromen-2-yl)phenoxy)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-83-1
(2-hydroxyethyl)(methyl)amine

: 1352306-13-8
2-(4-iodophenyl)-4-methyl-6-((tetrahydro-2H-pyran-2-yl)oxy)-3-(3-((tetrahydro-2H-pyran-2-yl)oxy)phenyl)-2H-chromene

: 1352306-74-1
N-methyl-2-(4-(4-methyl-6-((tetrahydro-2H-pyran-2-yl)oxy)-3-(3-((tetrahydro-2H-pyran-2-yl)oxy)phenyl)-2H-chromen-2-yl)phenoxy)ethanamine

: C₃₅H₄₁NO₆

Guidance literature:: With caesium carbonate; copper(l) iodide; In propyl cyanide; at 125 ℃; for 4h; Inert atmosphere;

Reference yield:

: 17918-14-8
2,5-dimethoxybenzoyl chloride

: 1352306-74-1
N-methyl-2-(4-(4-methyl-6-((tetrahydro-2H-pyran-2-yl)oxy)-3-(3-((tetrahydro-2H-pyran-2-yl)oxy)phenyl)-2H-chromen-2-yl)phenoxy)ethanamine

: C₃₅H₄₁NO₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C

2.1: magnesium / iodine / tetrahydrofuran / 1.75 h / 60 °C

2.2: 1 h / 0 °C

3.1: boron tribromide / dichloromethane / 0.5 h / -78 - 0 °C

3.2: -78 °C

4.1: pyridinium p-toluenesulfonate / dichloromethane / 1 h / 20 °C

5.1: piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene / 2-methyl-propan-1-ol / 1.5 h / Dean-Stark trap; Reflux

6.1: tetrahydrofuran / 2.25 h / 0 - 20 °C

6.2: 0 °C

7.1: water; acetic acid / tetrahydrofuran / 90 °C

8.1: pyridinium p-toluenesulfonate / dichloromethane / 3 h / 20 °C

9.1: caesium carbonate / copper(l) iodide / propyl cyanide / 4 h / 125 °C / Inert atmosphere

With piperidine; water; boron tribromide; caesium carbonate; magnesium; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; copper(l) iodide; iodine; pyridinium p-toluenesulfonate; In tetrahydrofuran; propyl cyanide; dichloromethane; 2-methyl-propan-1-ol;

Reference yield:

: 1352306-15-0
3-(3-hydroxyphenyl)-2-(4-iodophenyl)-4-methyl-2H-chromen-6-ol

: 1352306-74-1
N-methyl-2-(4-(4-methyl-6-((tetrahydro-2H-pyran-2-yl)oxy)-3-(3-((tetrahydro-2H-pyran-2-yl)oxy)phenyl)-2H-chromen-2-yl)phenoxy)ethanamine

: C₃₅H₄₁NO₆

Guidance literature:: Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate / dichloromethane / 3 h / 20 °C

2: caesium carbonate / copper(l) iodide / propyl cyanide / 4 h / 125 °C / Inert atmosphere

With caesium carbonate; copper(l) iodide; pyridinium p-toluenesulfonate; In propyl cyanide; dichloromethane;