5-ethyl-2,3,4-trimethoxy-12-(p-tolyl)-11,12-dihydro-5H-5,12-diazabenzo[5,6]pentaleno[2,1-b]naphthalen-6-one

Base Information

Chemical Name:5-ethyl-2,3,4-trimethoxy-12-(p-tolyl)-11,12-dihydro-5H-5,12-diazabenzo[5,6]pentaleno[2,1-b]naphthalen-6-one
CAS No.:1619937-44-8
Molecular Formula:C₃₀H₂₈N₂O₄
Molecular Weight:480.563
Hs Code.:

Synonyms:5-ethyl-2,3,4-trimethoxy-12-(p-tolyl)-11,12-dihydro-5H-5,12-diazabenzo[5,6]pentaleno[2,1-b]naphthalen-6-one

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Chemical Property of 5-ethyl-2,3,4-trimethoxy-12-(p-tolyl)-11,12-dihydro-5H-5,12-diazabenzo[5,6]pentaleno[2,1-b]naphthalen-6-one

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Technology Process of 5-ethyl-2,3,4-trimethoxy-12-(p-tolyl)-11,12-dihydro-5H-5,12-diazabenzo[5,6]pentaleno[2,1-b]naphthalen-6-one

There total 4 articles about 5-ethyl-2,3,4-trimethoxy-12-(p-tolyl)-11,12-dihydro-5H-5,12-diazabenzo[5,6]pentaleno[2,1-b]naphthalen-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1619937-24-4
2-(2-bromobenzyl)-5-ethyl-7,8,9-trimethoxy-1-(p-tolyl)-1,5-dihydropyrrolo[3,2-c]quinolin-4-one

: 1619937-44-8
5-ethyl-2,3,4-trimethoxy-12-(p-tolyl)-11,12-dihydro-5H-5,12-diazabenzo[5,6]pentaleno[2,1-b]naphthalen-6-one

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; In toluene; at 120 ℃; for 16h; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.tet.2014.05.084

Reference yield: 67.0%

: 1619937-17-5
2-benzyl-5-ethyl-7,8,9-trimethoxy-1-(p-tolyl)-1H-pyrrolo[3,2-c]quinolin-4(5H)-one

: 1619937-44-8
5-ethyl-2,3,4-trimethoxy-12-(p-tolyl)-11,12-dihydro-5H-5,12-diazabenzo[5,6]pentaleno[2,1-b]naphthalen-6-one

Guidance literature:: With copper diacetate; palladium diacetate; Trimethylacetic acid; In toluene; at 140 ℃; for 20h; Sealed tube;
DOI:10.1016/j.tet.2014.05.084

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 1619937-44-8
5-ethyl-2,3,4-trimethoxy-12-(p-tolyl)-11,12-dihydro-5H-5,12-diazabenzo[5,6]pentaleno[2,1-b]naphthalen-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / 1,2-dichloro-ethane / 16 h / 105 °C / Inert atmosphere

2: palladium diacetate; copper diacetate; Trimethylacetic acid / toluene / 20 h / 140 °C / Sealed tube

With copper diacetate; palladium diacetate; toluene-4-sulfonic acid; Trimethylacetic acid; In 1,2-dichloro-ethane; toluene;
DOI:10.1016/j.tet.2014.05.084