(S)-3-Methylpentadecyl tosylate

Base Information

Chemical Name:(S)-3-Methylpentadecyl tosylate
CAS No.:130797-63-6
Molecular Formula:C₂₃H₄₀O₃S
Molecular Weight:396.635
Hs Code.:

Synonyms:(S)-3-Methylpentadecyl tosylate

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Chemical Property of (S)-3-Methylpentadecyl tosylate

Chemical Property:

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Technology Process of (S)-3-Methylpentadecyl tosylate

There total 10 articles about (S)-3-Methylpentadecyl tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 130797-61-4
(S)-3-Methyl-1-pentadecanol

: 98-59-9
p-toluenesulfonyl chloride

: 130797-63-6
(S)-3-Methylpentadecyl tosylate

Guidance literature:: With pyridine; at 0 - 5 ℃; for 12h;

Reference yield:

: 5949-05-3
(S)-Citronellal

: 130797-63-6
(S)-3-Methylpentadecyl tosylate

Guidance literature:: Multi-step reaction with 10 steps

1: lithium aluminium tetrahydride / diethyl ether

2: potassium tert-butylate / dimethyl sulfoxide

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane

4: periodic acid dihydrate / diethyl ether; tetrahydrofuran / 1 h / 0 - 20 °C

5: lithium aluminium tetrahydride / diethyl ether

6: pyridine

7: sodium iodide / N,N-dimethyl-formamide

8: n-butyllithium; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / Reflux

9: palladium 10% on activated carbon; hydrogen; acetic acid

10: pyridine

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; n-butyllithium; periodic acid dihydrate; palladium 10% on activated carbon; potassium tert-butylate; hydrogen; acetic acid; 3-chloro-benzenecarboperoxoic acid; sodium iodide; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1271/bbb.120436

Reference yield:

: 67245-14-1,138524-35-3,138524-41-1
(3S,6RS)-1-benzyloxy-6,7-epoxy-3,7-dimethyloctane

: 130797-63-6
(S)-3-Methylpentadecyl tosylate

Guidance literature:: Multi-step reaction with 7 steps

1: periodic acid dihydrate / diethyl ether; tetrahydrofuran / 1 h / 0 - 20 °C

2: lithium aluminium tetrahydride / diethyl ether

3: pyridine

4: sodium iodide / N,N-dimethyl-formamide

5: n-butyllithium; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / Reflux

6: palladium 10% on activated carbon; hydrogen; acetic acid

7: pyridine

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; n-butyllithium; periodic acid dihydrate; palladium 10% on activated carbon; hydrogen; acetic acid; sodium iodide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1271/bbb.120436