C₃₀H₄₃NO₁₀S₂

Base Information

Chemical Name:C₃₀H₄₃NO₁₀S₂
CAS No.:678156-21-3
Molecular Formula:C₃₀H₄₃NO₁₀S₂
Molecular Weight:641.804
Hs Code.:

C<sub>30</sub>H<sub>43</sub>NO<sub>10</sub>S<sub>2</sub>

Synonyms:C₃₀H₄₃NO₁₀S₂

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Chemical Property of C₃₀H₄₃NO₁₀S₂

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Technology Process of C₃₀H₄₃NO₁₀S₂

There total 13 articles about C₃₀H₄₃NO₁₀S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 98-59-9
p-toluenesulfonyl chloride

: 678156-20-2
[(S)-5-Hydroxy-1-((4S,5S)-5-hydroxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-pentyl]-carbamic acid tert-butyl ester

: 678156-21-3
C₃₀H₄₃NO₁₀S₂

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/j.tet.2019.130496

Reference yield:

: 111-29-5
1 ,5-pentanediol

: 678156-21-3
C₃₀H₄₃NO₁₀S₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: 80 percent / NaH

2.1: 80 percent / PCC

3.1: LDA / hexane; tetrahydrofuran / 1 h / -78 °C

3.2: 70 percent / tetrahydrofuran; hexane / 3 h / -78 °C

4.1: 91 percent / ZnCl₂; DIBAL-H / tetrahydrofuran; toluene / 0.67 h / -78 °C

5.1: 85 percent / H₂O; N-bromosuccinimide / toluene / 0.25 h / 20 °C

6.1: 83 percent / K₂CO₃ / methanol / 1.75 h / 0 - 20 °C

7.1: 85 percent / NH₄Cl; NaN₃ / methanol; H₂O / 6 h / Heating

8.1: 87 percent / CSA / acetone / 1 h / 20 °C

9.1: Et₃N / CH₂Cl₂ / 0.25 h / 0 °C

10.1: 0.50 g / NaBH₄; aq. NaHCO₃ / CH₂Cl₂ / 0.33 h / 0 °C

11.1: 82 percent / H₂ / Pd(OH)2 / ethanol / 16 h / 20 °C / atmospheric pressure

12.1: 75 percent / Et₃N / CH₂Cl₂ / 1 h

With sodium tetrahydroborate; N-Bromosuccinimide; sodium azide; camphor-10-sulfonic acid; water; hydrogen; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; ammonium chloride; triethylamine; pyridinium chlorochromate; zinc(II) chloride; lithium diisopropyl amide; palladium dihydroxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; acetone; toluene; 10.1: Pummerer reaction;
DOI:10.1016/j.tetasy.2003.12.017

Reference yield:

: 115463-10-0
ethyl (E)-7-(benzyloxy)hept-2-enoate

: 678156-21-3
C₃₀H₄₃NO₁₀S₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: LDA / hexane; tetrahydrofuran / 1 h / -78 °C

1.2: 70 percent / tetrahydrofuran; hexane / 3 h / -78 °C

2.1: 91 percent / ZnCl₂; DIBAL-H / tetrahydrofuran; toluene / 0.67 h / -78 °C

3.1: 85 percent / H₂O; N-bromosuccinimide / toluene / 0.25 h / 20 °C

4.1: 83 percent / K₂CO₃ / methanol / 1.75 h / 0 - 20 °C

5.1: 85 percent / NH₄Cl; NaN₃ / methanol; H₂O / 6 h / Heating

6.1: 87 percent / CSA / acetone / 1 h / 20 °C

7.1: Et₃N / CH₂Cl₂ / 0.25 h / 0 °C

8.1: 0.50 g / NaBH₄; aq. NaHCO₃ / CH₂Cl₂ / 0.33 h / 0 °C

9.1: 82 percent / H₂ / Pd(OH)2 / ethanol / 16 h / 20 °C / atmospheric pressure

10.1: 75 percent / Et₃N / CH₂Cl₂ / 1 h

With sodium tetrahydroborate; N-Bromosuccinimide; sodium azide; camphor-10-sulfonic acid; water; hydrogen; diisobutylaluminium hydride; sodium hydrogencarbonate; potassium carbonate; ammonium chloride; triethylamine; zinc(II) chloride; lithium diisopropyl amide; palladium dihydroxide; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; water; acetone; toluene; 7.1: Pummerer reaction;
DOI:10.1016/j.tetasy.2003.12.017