tert-butyl 4-(2-phenyl-9H-benzo[f]imidazo[1,2-d]pyrido[2,3-b][1,4]diazepin-3-yl)benzylcarbamate

Base Information

Chemical Name:tert-butyl 4-(2-phenyl-9H-benzo[f]imidazo[1,2-d]pyrido[2,3-b][1,4]diazepin-3-yl)benzylcarbamate
CAS No.:1374262-89-1
Molecular Formula:C₃₂H₂₉N₅O₂
Molecular Weight:515.615
Hs Code.:

Synonyms:tert-butyl 4-(2-phenyl-9H-benzo[f]imidazo[1,2-d]pyrido[2,3-b][1,4]diazepin-3-yl)benzylcarbamate

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Chemical Property of tert-butyl 4-(2-phenyl-9H-benzo[f]imidazo[1,2-d]pyrido[2,3-b][1,4]diazepin-3-yl)benzylcarbamate

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Technology Process of tert-butyl 4-(2-phenyl-9H-benzo[f]imidazo[1,2-d]pyrido[2,3-b][1,4]diazepin-3-yl)benzylcarbamate

There total 5 articles about tert-butyl 4-(2-phenyl-9H-benzo[f]imidazo[1,2-d]pyrido[2,3-b][1,4]diazepin-3-yl)benzylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 489446-42-6
4-((tert-butoxycarbonylamino)methyl)phenylboronic acid

: 1374262-88-0
3-bromo-2-phenyl-9H-benzo[f]imidazo[1,2-d]pyrido[2,3-b][1,4]diazepine

: 1374262-89-1
tert-butyl 4-(2-phenyl-9H-benzo[f]imidazo[1,2-d]pyrido[2,3-b][1,4]diazepin-3-yl)benzylcarbamate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate; In ethanol; water; toluene; at 100 ℃; Inert atmosphere;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 1374262-89-1
tert-butyl 4-(2-phenyl-9H-benzo[f]imidazo[1,2-d]pyrido[2,3-b][1,4]diazepin-3-yl)benzylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / ISOPROPYLAMIDE; mineral oil / 0 - 20 °C

1.2: 2 h / 0 - 20 °C

2.1: ammonium acetate; acetic acid / 3 h / 120 °C

3.1: N-Bromosuccinimide / tetrahydrofuran / 1 h / 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / ethanol; water; toluene / 100 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium acetate; sodium hydride; sodium hydrogencarbonate; acetic acid; In tetrahydrofuran; ethanol; ISOPROPYLAMIDE; water; toluene; mineral oil;

Reference yield:

: 885-70-1
5H-benzo[e]pyrido[3,2-b][1,4]diazepin-6(11H)-one

: 1374262-89-1
tert-butyl 4-(2-phenyl-9H-benzo[f]imidazo[1,2-d]pyrido[2,3-b][1,4]diazepin-3-yl)benzylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / ISOPROPYLAMIDE; mineral oil / 0 - 20 °C

1.2: 2 h / 0 - 20 °C

2.1: ammonium acetate; acetic acid / 3 h / 120 °C

3.1: N-Bromosuccinimide / tetrahydrofuran / 1 h / 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate / ethanol; water; toluene / 100 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium acetate; sodium hydride; sodium hydrogencarbonate; acetic acid; In tetrahydrofuran; ethanol; ISOPROPYLAMIDE; water; toluene; mineral oil;